effect of high temperature treatment on aqueous corrosion of low-carbon steel by electrochemical impedance spectroscopy高温处理对水的影响腐蚀电化学阻抗谱的低碳钢.pdfVIP

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effect of high temperature treatment on aqueous corrosion of low-carbon steel by electrochemical impedance spectroscopy高温处理对水的影响腐蚀电化学阻抗谱的低碳钢.pdf

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effect of high temperature treatment on aqueous corrosion of low-carbon steel by electrochemical impedance spectroscopy高温处理对水的影响腐蚀电化学阻抗谱的低碳钢

Materials Sciences and Applications, 2011, 2, 81-86 81 doi:10.4236/msa.2011.22011 Published Online February 2011 (http://www.SciRP.org/journal/msa) Effect of High Temperature Treatment on Aqueous Corrosion of Low-Carbon Steel by Electrochemical Impedance Spectroscopy* 1 1 2 Samuel J. Gana , Nosa O. Egiebor , Ramble Ankumah 1Environmental Engineering Program, Chemical Engineering Department, Tuskegee University, Tuskegee, USA; 2Department of Agricultural and Environmental Sciences, Tuskegee University, Tuskegee, USA. Email: Egiebor@ Received December 28th, 2010; revised January 11th, 2011; accepted January 16th, 2011. ABSTRACT The corrosion behavior of 1020C carbon steel samples that had been subjected to oxidizing heat treatment at 550˚C and 675˚C were studied in sodium chloride electrolytes using a 3-electrode electrochemical impedance spectroscopy. Experimental data were used to evaluate the corrosion behavior of the samples while optical microscopy was employed to investigate the surface characteristics of the samples before and after aqueous corrosion. The results showed that while the sample treated at 550˚C revealed an increasing corrosion rate with time, the sample treated at 675˚C indi- cated a higher initial corrosion rate, but the rate declined gradually over the 4-day experimental period. Optical mi- croscopy revealed significant formation of surface corrosion products on both heat treated samples, but the complex plane diagrams indicated significant capacitive behavior for the heat treated samples relative to the untreated samples. Keywords : Impedance, Carbon Steel, Corrosion, Nyquist Diagrams, Photomicrographs 1. Introduction perature.