液相法制备MoO3纳米结构.docVIP

液相法制备MoO3纳米结构 摘要 “纳米”是一个长度单位，1纳米是1米的十亿分之一(1nm=10-9m）相当于头发丝直径的十万分之一。纳米材料指的是晶粒尺寸为纳米级(10-9m)的超细材料。纳米材料由于具有与块体材料不同的尺寸效应、体积 效应、表面界面效应和宏观量子隧道效应等，使其在电子信息、化工、生物工程、医药、航空航天、国防等高尖端领域有着广泛的应用前景。纳米材料既是一种新材料又是构成新材料的重要原料。 钼和钼合金材料不仅具有良好的耐高温强度和硬度,而且具有良好的导电、导热、抗腐蚀等性能,此广泛应用于化学化工、冶金机械及航空航天等工业领域。三氧化钼( MoO3) 不仅是制备钼和钼合金材料的主要原料,而且本身也具有电致变色、光致变色、光催化降解及气敏等特性, 因此在合成敏感元件、催化剂、快离子导体及潜在的电池电极等许多功能材料方面具有特殊用途。 制备性能优异的三氧化钼薄膜一直是研究的重点。近年来,随着科学技术的进步,不断出现许多新型的三氧化钼薄膜制备方法。目前已有多种制备MoO3 薄膜的方法,如蒸镀法、电化学沉积法 、溅射法、溶胶-凝胶法等。本文主要从沉淀法，水热法，化学气象沉积法，溶胶凝胶法等工艺流程来阐述MoO3的制备。 关键词:纳米,三氧化钼,液相法,纳米薄膜,钼合金材料 LIQUID PHASE PREPARATION OF NANO MoO3 ABSTRACT Nano is a unit of length, 1 nanometer is one hundred billionth of a meter (1 nm = 10-9 m), and it is equivalent to one over one hundred thousand the diameter of a hair. Nano material refers to the grain size for the nanometer level (10-9 m) of super fine material. Because of Nano materials have different size effect, surface effect, volume interface effect and macro scopical quantum tunnel effect etc, when compared with bulk materials, making Nano materials have a wide range of applications in electronic information industry, chemical industry, biological engineering, medicine, aviation, frontier defense etc. Nano material is not only a kind of new material but also an important raw material of the new material. Molybdenum and molybdenum alloy material not only has good resistance to high temperature and good hardness strength, but also has good electric conductivity, thermal conductivity, corrosion resistance and other properties, they are widely used in chemical industry, metallurgy mechanical , aerospace and other industries. Three molybdenum oxide (MoO3) is not only the main raw material to make molybdenum and molybdenum alloy material, meanwhile it also has the effect of electro chromic, photo chromic, photo catalytic degradation and characteristics of air sensitive, what’s more, it has special use in many functional materials with different purposes ,such as the synt