氟离子选择电极法测定砖茶中氟含量的稳定性研究-食品安全质量检测.PDF

4 4 Vol. 4 No. 4 2013 8 Journal of Food Safety and Quality Aug. , 2013 1, 2 1, 2 1 2 1, 2* 李戎娟 , 刘东娜 , 李 俊 , 魏晓惠 , 杜 晓 (1. (), 625014; 2. (), 625014) 摘 要: 目的 , 方法 , 结果 (TISAB), 120 g/L(TISAB-2), (TISAB-GB); 0.25 g , , 490.73±6.36 mg/kg, ; ; ; 结论 , , , , 关键词: ; ; ; Stability of fluoride ion selective electrode method to detect fluorine content in brick tea 1, 2 1, 2 1 2 1, 2* LI Rong-Juan , LIU Dong-Na , LI Jun , WEI Xiao-Hui , DU Xiao (1. RD Center, National Tea Inspection Center (Sichuan), Sichuan Agricultural University, Ya’an 625014, China; 2. National Tea Quality Inspection Center (Sichuan), Ya’an 625014, China) ABSTRACT: Objective To explore the stability of fluoride ion selective electrode method to detect fluorine content in brick tea, and provide theoretical data for its calibration. Methods Samples were extracted by boiling water, using TISAB buffer solution to eliminate the effect of interfering ions and acidity, and then measured by fluoride ion selective electrode. Results The factors had an obvious