堆肥处理对污泥腐殖物质组成和光谱学特征的影响-环境化学.PDFVIP

23 1 Vol. 23, No. 1 2004 1 ENVIRONMENTAL CHEMISTRY January 2004 * 1 2 1* * 张雪英 黄焕忠 周立祥 ( 1 , , 210095; 2 ) (Sephadex G75) HA FA . , 63d , HA ; FA , , , FA 30% , . , : , HA , ; FA . , , , . . , [ 1] . , ( , FA) ( , HA) , , . ( ) , HA FA , . 1 11 ( ) ( 11) , 3 1 1 035m t min 63d . 3 , ( 55, 70) , 8d. (0d) ( 63d) , . 12 HA FA . 1 ( 63d) , 01moll HCl 110 ( 2002 11 3 . * ( RBF/ 1998) ( BS2000009) . * * 1 : 97 pH 1 2 ) , 1h, ( 17000g) . 045m FA1 , FA1. 1 NaOH pH= 7, N 01moll NaOH 2 110, 4h, . ( 17000g) 045m . 1 60moll HCl pH 1 2 , , ( 17000g) (HA 1 1 ) ( FA ) . HA 01moll HCl 03moll HF . 2 ( MilliQ) , 8000Da , Cl . FA FA 1000Da 1 2 HCl 24h . HA FA. 13 HA FA Sephadex G75 ( 303ml, 67cm, 25mm) . 10ml HA FA , pH= 68 1 (MilliQ) , 10mlmin , 5ml . 10ml Dextran Blue2000 ( 2%) ( V ) 0 100ml. 280nm ( Shimadze UN1601UV/VIS spectrophotometer) , . 10mg HA FA 10ml (milliQ) , 1 15min , , Whatman No2 , 005moll NaOH [2] pH= 80 . 10nm, 1 120nmmin . 380nm 550nm, 360nm, 270nm