年产500吨丁基丙二酸二乙酯反应釜的设计.docVIP

年产500吨丁基丙二酸二乙酯反应釜的设计 摘要：设计任务是设计年产500吨丁基丙二酸二乙酯的反应釜，利用相转移催化法，设计了带有夹套的搅拌型反应釜，最终实现了预定的产量目标。本设计依据国家相关标准、规范对中搅拌式反应釜进行了强度和刚度设计，并且对反应釜的整体结构、标准零部件的选型、非标准件的结构和选材进行了优化设计。本文按照给定的工艺参数对筒体、封头、及开孔补强等进行了系统的强度计算，校核了它们的刚度；并根据给定的换热面积，确定了釜体夹套的高度。以此为依据进行了施工图的设计。本设备的设计、制造接受国家质量技术监督局《压力容器安全技术监察规程》的监察。本次设计提高了运用标准规范和查阅文献资料的能力，为今后的工程设计奠定了良好的基础。10911 关键词：丁基丙二酸二乙酯；反应釜；结构 The Design of Reactor for an Annual Output of 500t Diethyln-butylmalonate Abstract: The design task is to design an annual output of 500t Diethyln-butylmalonate reactor, which is using of phase transfer catalysis. Ultimately, a jacketed stirred reactor is designed, and the intended production target is achieved. This design based on related standards, norms to stir type reaction axe in the strength and stiffness of the reaction kettle design, and the structure of the components of the selection of the standard, non-standard, the structure of the material and the optimization design. This paper according to a given process parameters on the cylinder body, sealing head, and open hole to fill strong of strength calculation system, check their stiffness, and according to the given heat transfer area, make sure the axe body clip the height of the set. Based on the design of the construction drawing. This equipment in the design, manufacture to receive the national quality technology supervision bureau quot;pressure vessel safety technology and inspection rules for monitoring. This design by using the standard and improve the ability of the literature review, the engineering design for the future to lay a good foundation. 3.1.7 内筒及夹套的受力分析13 3.1.8 计算夹套筒体、封头厚度13 3.1.9 计算内筒筒体厚度14 3.1.10 确定内筒封头厚度14 3.2 反应釜的搅拌装置15 3.2.1 确定搅拌器的型式15 3.2.2 确定搅拌轴系15 3.2.3 确定搅拌附件17 3.3 反应釜的传动装置17 3.3.1 确定电动机17 3.3.2 确定减速机17 3.3.2 确定传动装置的机座18 3.3.4 底座设计18 3.4 反应釜的轴封装置19 3.4.1 确定轴封类型19 3.4.2 确定轴封装置型号19 3.5 反应釜的附件设计20 3.5.1 法兰联接结构设计20 3.5.2 人孔的设计21 3.5.3 视镜的设计21 4 结论22 致谢23 参考文献24 1 引言 1.1 丙二酸二乙酯的性质和用途 1.1.1 丙二酸二乙酯的性质 丙二酸二乙酯(DEM)，又称胡萝卜酸乙酯，其结构式为: 丙二酸二乙酯的纯