分光光度法测定复方天麻颗粒中甘油磷酸钠的含量（Determination of sodium phosphate in compound Tianma granules by Spectrophotometry）.docVIP

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分光光度法测定复方天麻颗粒中甘油磷酸钠的含量（Determination of sodium phosphate in compound Tianma granules by Spectrophotometry）.doc

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分光光度法测定复方天麻颗粒中甘油磷酸钠的含量（Determination of sodium phosphate in compound Tianma granules by Spectrophotometry）

分光光度法测定复方天麻颗粒中甘油磷酸钠的含量（Determination of sodium phosphate in compound Tianma granules by Spectrophotometry） Determination of sodium phosphate in compound Tianma granules by Spectrophotometry Rong Rong 1* Chen Mingqiang 1 Yang Yong 2 1 1 (1 fake Li Hongxiao natural medicine Shandong University of Traditional Chinese Medicine Key Laboratory of Shandong University of Traditional Chinese Medicine; 2 molecular and cell biology laboratory, Shandong Jinan 250014) Compound Tianma Granule is used to treat vertigo, mental exhaustion and neurasthenia caused by dysfunction of efferent nerve. Sodium phosphate is a supplement to the formula. P involved in bone formation, which involved in cell membrane phospholipid form, related enzyme activity and phosphorus and many metabolism, plays a crucial role in energy metabolism; for the adjuvant treatment of efferent nerve dysfunction caused by dizzy, mental fatigue, neurasthenia and other diseases. Therefore, it is one of the keys to control the quality of the compound to determine the content of the sodium glycerin phosphate in it and establish its quality standard. The content of the standard of the original preparation is not determined; the reference content of the Peoples Republic of China Pharmacopoeia, 2005 edition, two parts and related references [1,2] is established, and the content of sodium phosphate is controlled by spectrophotometry. 1 experimental part 1.1 instrument and reagent HITACHI 2800 UV visible spectrophotometer (Hitachi, Japan); SX2-1-10 box type resistance furnace (Shandong province Longkou City electric furnace factory); Mettler 240 AE electronic balance (Swiss Mettler company). Beta glycerophosphate (C3H7Na2O6P, 5H2O, Fluka, No. 50020); potassium dihydrogen phosphate (Chinese Institute for drug control, batch 100745-200401); water deionized water; other reagents were analytical grade. 1.2 test method Preparation of 1.2.1 solution The sample solution preparation batch of compound Tianma Granule, 050422 porphyri