preparation of a carbon-based solid acid catalyst by sulfonating activated carbon in a chemical reduction process碳基固体酸催化剂的制备磺化活性炭在化学还原法.pdfVIP

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preparation of a carbon-based solid acid catalyst by sulfonating activated carbon in a chemical reduction process碳基固体酸催化剂的制备磺化活性炭在化学还原法.pdf

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preparation of a carbon-based solid acid catalyst by sulfonating activated carbon in a chemical reduction process碳基固体酸催化剂的制备磺化活性炭在化学还原法

Molecules 2010, 15, 7188-7196; doi:10.3390/molecule OPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Article Preparation of a Carbon-Based Solid Acid Catalyst by Sulfonating Activated Carbon in a Chemical Reduction Process Xiao-Yan Liu 1, Miao Huang 1, Hai-Long Ma 1,*, Zeng-Qiang Zhang 1, Jin-Ming Gao 1, 2 2 2 Yu-Lei Zhu , Xiao-Jin Han and Xiang-Yun Guo 1 College of Science, Northwest AF University, Yangling 712100, Shaanxi, China 2 State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, CAS, Taiyuan 030001, China * Author to whom correspondence should be addressed; E-Mails: mahl@ or mahl1979@; Tel.: +86-29 Fax: +86-29 Received: 14 September 2010; in revised form: 11 October 2010 / Accepted: 13 October 2010 / Published: 18 October 2010 Abstract: Sulfonated (SO H-bearing) activated carbon (AC-SO H) was synthesized by an 3 3 aryl diazonium salt reduction process. The obtained material had a SO H density of 3 -1 2 -1 0.64 mmol·g and a specific surface area of 602 m ·g . The catalytic properties of AC- SO3H were compared with that of two commercial solid acid catalysts, Nafion NR50 and Amberlyst-15. In a 10-h esterification reacti