preparation of superhydrophobic polymeric film on aluminum plates by electrochemical polymerization制备超疏水聚合物薄膜上通过电化学聚合铝盘子.pdfVIP

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preparation of superhydrophobic polymeric film on aluminum plates by electrochemical polymerization制备超疏水聚合物薄膜上通过电化学聚合铝盘子.pdf

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preparation of superhydrophobic polymeric film on aluminum plates by electrochemical polymerization制备超疏水聚合物薄膜上通过电化学聚合铝盘子

Molecules 2009, 14, 4737-4746; doi:10.3390/molecule OPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Article Preparation of Superhydrophobic Polymeric Film on Aluminum Plates by Electrochemical Polymerization Fang Wang *, Heyi Luo, Qian Wang, Jinggang Wang and Juan Xu College of Science, Northwest Agriculture Forest University, Xinong Road No.22, Yangling, Shanxi, 712100, China; E-Mail: liurenzu@ (J.X.) * Author to whom correspondence should be addressed: E-Mail: wf4070@ or wangfang4070@; Tel.: +86-29-870-922-26; Fax: +86-29-870-920-82. Received: 15 October 2009; in revised form: 16 November 2009; / Accepted: 19 November 2009 / Published: 19 November 2009 Abstract: 6-(N-Allyl-1,1,2,2-tetrahydroperfluorododecyl)amino-1,3,5-triazine-2,4-dithiol monosodium (ATP) was used to prepare polymeric thin films on pure aluminum plates to achieve a superhydrophobic surface. The electrochemical polymerization process of ATP on aluminum plates in NaNO2 aqueous solution and the formation of poly(6-(N-allyl- 1,1,2,2-tetrahydroperfluorododecyl)amino-1,3,5-triazine-2,4-dithiol) (PATP) thin film were studied by means of optical ellipsometry and film weight. The chemical structure of the polymeric film is investigated using FT-IR spectra and X-ray photoelectron spectroscopy (XPS). Contact angle goniometry was applied to measure the contact angles with distilled water drops at ambient temperature. The experimental results indicate that the polymeric film formed on pure alumin