response behaviour of a hydrogen sensor based on ionicconducting polymer-metal interfaces prepared by the chemicalreduction method氢气传感器的响应行为基于ionicconducting高分子金属接口由chemicalreduction方法.pdfVIP

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response behaviour of a hydrogen sensor based on ionicconducting polymer-metal interfaces prepared by the chemicalreduction method氢气传感器的响应行为基于ionicconducting高分子金属接口由chemicalreduction方法.pdf

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response behaviour of a hydrogen sensor based on ionicconducting polymer-metal interfaces prepared by the chemicalreduction method氢气传感器的响应行为基于ionicconducting高分子金属接口由chemicalreduction方法

Sensors 2006, 6, 284-297 sensors ISSN 1424-8220 © 2006 by MDPI /sensors Response Behaviour of a Hydrogen Sensor Based on Ionic Conducting Polymer-metal Interfaces Prepared by the Chemical Reduction Method * * Mariappan Sakthivel and Werner Weppner Chair for Sensors and Solid State Ionics, Faculty of Engineering, Christian Albrechts University, Kaiserstraße 2, D-24143 Kiel, Germany * Authors to whom correspondence should be addressed. Email: msa@tf.uni-kiel.de, ww@tf.uni-kiel.de Received: 26 July 2005 / Accepted: 28 February 2006 / Published: 7 April 2006 Abstract: A solid-state amperometric hydrogen sensor based on a protonated Nafion membrane and catalytic active electrode operating at room temperature was fabricated and tested. Ionic conducting polymer-metal electrode interfaces were prepared chemically by using the impregnation-reduction method. The polymer membrane was impregnated with tetra-ammine platinum chloride hydrate and the metal ions were subsequently reduced by using either sodium tetrahydroborate or potassium tetrahydroborate. The hydrogen sensing characteristics with air as reference gas is reported. The sensors were capable of detecting hydrogen concentrations from 10 ppm to 10% in nitrogen. The response time was in the range of 10-30 s and a stable linear current output was observed. The thin Pt films were characterized by XRD