screening for γ-nonalactone in the headspace of freshly cooked non-scented rice using spmegc-o and spmegc-ms筛查γ-nonalactone顶部空间的新鲜煮熟水稻使用spmegc-o和spmegc-ms没有用.pdfVIP
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screening for γ-nonalactone in the headspace of freshly cooked non-scented rice using spmegc-o and spmegc-ms筛查γ-nonalactone顶部空间的新鲜煮熟水稻使用spmegc-o和spmegc-ms没有用
Molecules 2009, 14, 2927-2934; doi:10.3390/molecule
OPEN ACCESS
molecules
ISSN 1420-3049
/journal/molecules
Communication
Screening for γ-Nonalactone in the Headspace of Freshly
Cooked Non-Scented Rice Using SPME/GC-O and
SPME/GC-MS
Zhi Zeng 1, Han Zhang 2,*, Tao Zhang 3, Shigeru Tamogami 2 and Jie Yu Chen 2
1 School of Chemistry and Environment, South China Normal University, Guangzhou 510631, China;
E-mail: zhizeng@ (Z.Z.)
2 Faculty of Bioresource Sciences, Akita Prefectural University, Kaidobata-Nishi 241-438,
Shimoshinjo-Nakano, Akita-shi, Akita 010-0195, Japan
3 Institute of Opto-electronic Materials and Technology, South China Normal University, Guangzhou
510631, China
* Author to whom correspondence should be addressed; E-mail: zhangh@akita-pu.ac.jp
Received: 22 June 2009; in revised form: 13 July 2009 / Accepted: 27 July 2009 /
Published: 10 August 2009
Abstract: The determination of γ-nonalactone as one of the important odor-active
compounds in freshly cooked non-scented rice is reported. It was evaluated by gas
chromatography-olfactometry (GC-O) analysis and identified by gas chromatography-mass
spectrometry (GC-MS) analysis in the headspace above the freshly cooked non-scented
rice samples extracted by using a modified headspace solid-phase microextraction (SPME)
method. This component had a mass spectrum with a characteristic ion peak at m/z 85
(100%) and a linear retention index (RI) of 2,023 on a DB Wax column, consistent with
those of
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