(多孔)陶瓷科学、材料处理、力学有限元计算经典结合之作.pptVIP

* * * Crushable strength Characterization of Foams Compression Test SHIMATZU Universal Machine (Max. 10000 N) Crosshead speed 0.2mm/min compliance layer, rubber Compressive properties are doubtful: Young’s modulus is too small; Crushable strength is more trustworthy; The crush was too sudden for instrument to detect and caused risk of damage * Computed X-ray Tomography (CT) The v|tome|x ultra high-resolution CT, INSA Lyon France 3D Image Processing using AMIRA or AVIZO AMIRA: /amira-at-work.html; AVIZO: /vsg_prod_avizo_overview.php Principle of CT resolution * CT-Slice Image reconstruction 8 PPI foam 22 PPI foam Fig. 4.38: slice image of the 3D reconstructed structure of 30PPI ceramic foam The slice image illustrates the internal microstructure of ceramics struts, indicating the struts is hollow instead of being complete dense * CT-Reconstructed 3D structure 3D structure of 8PPI ceramic foam (42 mm x 21 mm x 19 mm) 3D structure of 22PPI ceramic foam (L14 mm x W13 mm x H8 mm) LCR Meter: HP4814A: 1000 Hz-1 MHz * Dielectric measurements e’’=wRC capacitance C in measured in pF by LCR, r is the radius of Au electrode of 5.6 mm, e0 is dielectric permittivity of vacuum (8.85x10-12 F/m). tand 0.02, excellent Ceramics with Gold electrode Sketch of setup * Dielectric constants Dielectric constant at RT The general behaviour for dielectric constant vs. frequency suggested a very stable performance from low up to high frequency and sensitive to sintering schedule The dielectric constant versus sintering schedule suggested that at 1350oC and longer lasting time gives lowest dielectric constant at 1 MHz; However the highest from 1250oC for 4h * Dielectric loss factor Dielectric loss at RT The general behaviour for dielectric loss versus frequency suggested an acceptable dielectric loss for real application (tand0.04);the doubt comes from measurement The dielectric constant versus sintering schedule suggested that at 1250oC and longer lasting time gives l