原创力文档synthesis of environmentally responsive polymers by atom transfer radical polymerization generation of reversible hydrophilic and hydrophobic surfaces环境响应性聚合物的合成原子转移自由基聚合生成的可逆的亲水和疏水表面.pdfVIP
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synthesis of environmentally responsive polymers by atom transfer radical polymerization generation of reversible hydrophilic and hydrophobic surfaces环境响应性聚合物的合成原子转移自由基聚合生成的可逆的亲水和疏水表面
Polymers 2010, 2, 40-56; doi:10.3390/polym2020040
OPEN ACCESS
Polymers
ISSN 2073-4360
/journal/polymers
Article
Synthesis of Environmentally Responsive Polymers by Atom
Transfer Radical Polymerization: Generation of Reversible
Hydrophilic and Hydrophobic Surfaces
Vikas Mittal 1,2
1 Department of Chemistry and Applied Biosciences, Institute of Chemical and Bioengineering,
ETH Zurich, Zurich, Switzerland; E-Mail: vikas.mittal@chem.ethz.ch
2 BASF SE, Polymer Research, 67056 Ludwigshafen, Germany
Received: 4 January 2010; in revised form: 11 March 2010 / Accepted: 27 April 2010 /
Published: 12 May 2010
Abstract: Environmentally responsive poly(N-isopropylacrylamide) brushes were grafted
from the surface of polymer particles or flat surfaces in order to generate reversible
hydrophilic and hydrophobic surfaces. The use of atom transfer radical polymerization was
demonstrated for the grafting of polymer brushes as it allows efficient control on the
amount of grafted polymer. The polymer particles were generated with or without
surfactant in the emulsion polymerization and their surface could be modified with the
atom transfer radical polymerization (ATRP) initiator. The uniform functionalization of the
surface with ATRP initiator was responsible for the uniform grafting of polymer brushes.
The grafted brushes responded reversibly with changes in temperature indicating that the
reversible responsive behavior could be tra
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