单分散纳米二氧化硅的制备与表征（Preparation and characterization of monodisperse nano silica）.doc

单分散纳米二氧化硅的制备与表征（Preparation and characterization of monodisperse nano silica） No. Volume 27 1 silicate bulletin Vol. 27, No. 1 2008 February BULLETIN, OF, THE, CHINESE, CERAMIC, SOCIETY February, 2008 Preparation and characterization of monodisperse nano silica Fuyuanxiang Sun Yanhui Xingxin, GE (School of chemistry and environment, South China Normal University Guangzhou 510006) abstract Use Stober sol 2 gel method The size of the composite was approximately Monodisperse nano silica spheres from 80 to 150nm The temperature and ammonia concentration were also discussed Degree as well as Effect of TEOS concentration on Synthesis of silica. utilize The samples were characterized by XRD, IR, SEM, TEM and other means. Result table bright The increase of hydrolysis temperature accelerates the maturation of silica particles in solution and induces agglomeration The increase of ammonia concentration results in an increase in nucleation rate Hydrolysis rate plus drama The particle size of silica increases The degree of agglomeration also increases. Increasing the amount of TEOS also results in a slight increase in the particle size of silica The degree of agglomeration is deepened. Key word Monodisperse Nanometer SiO2; sol 2 gel method CLC number : TQ127 FU, Yuan2xiang, SUN, Yan2hui, GE, X, ing2xin Document identifier : A article number : 100121625 (2008) 0120154206 SynthesisandCharacterization ofMonodisperseSiO 2Nanoparticles (SchoolofChemistryandEnvironment, SouthChinaNormalUniversity, Guangzhou510006, China) Abstract:, A, StOber, Sol2gelmethod, has, been, used, to, prepare, monodisperse, and, uniform, 2size, from,,... Nm silica nanoparticles in this paper. The silica particles were obtained by hydrolysis of tetraethyl Orthosilicate (TEOS) inethanolmediumuseammoniumascatalystandadetailedstudywascarriedout On, the, effect, of, different, temperature, amount, of, ammonium, and, TEOS, on,, particle, sizes, and, the Dispersion., The, structure, of, the, was, examined, by, XRD