滴定分析基本操作练习（Basic exercises for titrimetric analysis）.doc

滴定分析基本操作练习（Basic exercises for titrimetric analysis） Experiment three basic operation of titration analysis First, the purpose and requirements of the experiment 1. to master the preparation and use method of buret. 2. proficiency in correct titration operation. 3. master discoloration of methyl orange and phenolphthalein in near stoichiometric point, correctly determine the end point of titration. 4. after this experiment, reached the requirements: in 1 minutes with Vaseline; correct posture acid burette; method to determine the correct end point indicator master three methods; dripping solution: 1 drop wise; the one drop; the plus half drop. Two 、 experimental principle Titration analysis is a standard solution of an accurately known concentration in the sample solution is dripped into the burette, with just the stoichiometric relationship between the chemical reaction type standard solution until the amount of substance and the analyte amount of substance so far, it is a kind of method according to the concentration of standard solution and titration consumption calculation of the volume of sample analyte concentrations. The basic operations of titrimetric analysis include the choice of capacity, the proper use of the instrument, the determination and control of the end-point of titration, the reading of the titration data, the recording and processing of the titration, etc.. This experiment through acid-base titration, that is, between the strong acid and strong alkali titration to understand and learn the basic operation of titration analysis, for the future analysis of titration laid the foundation. The titration between a strong acid and a strong base is a titration based on acid base reaction, also called neutralization. When 0.1mol, L-1, HCl and 0.1 mol L-1 NaOH are titrated each other, the pH at the stoichiometric point is 7, and the range of pH jump in titration is 4.3 to 9.7, An indicator with color change in the range of jump can be used to ensure the a