生血胶囊的鉴别及含量测定（Identification and content determination of Sheng Xue capsule）.docVIP

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生血胶囊的鉴别及含量测定（Identification and content determination of Sheng Xue capsule）.doc

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生血胶囊的鉴别及含量测定（Identification and content determination of Sheng Xue capsule）

生血胶囊的鉴别及含量测定（Identification and content determination of Sheng Xue capsule） Identification and content determination of Sheng Xue capsule Update: 2009-11-23 Click: Wang Xu, van Lili, Zhou Furong Abstract: for the identification of pilose antler, calcined copperas microscopic identification, qualitative identification of Rhizoma Atractylodis by thin-layer chromatography, the calcined copperas was determined by spectrophotometric method. Results the corresponding microscopic features and thin spots can be detected from the samples. The content of ferrous sulfate has a good linear relationship (r=0.9999) in the range of 0.23 ~ 1.18mg, and the recovery is 100.73%. The method is simple, sensitive, reliable and practical. Keywords: @ Shengxue capsule / Chemistry / chemical; copperas; calcining; sulfate / analysis CLC number: R284.1, document identification code: A, article number: 1003-9783 (1999) 03-0180-02 Shengxue capsule from Atractylodes, calcined copperas, pilose antler, with Spleen Qi, kidney fill lean function, for iron deficiency, blood loss anemia treatment. In the calcined copperas as monarch drug, the main component of ferrous sulfate, the determination of ferrous ions by spectrophotometry. The antler and calcined copperas were qualitatively identified by microscopic identification, qualitative identification of Rhizoma Atractylodis by thin-layer chromatography, can comprehensively control the quality of drugs. 1 instruments, drugs and reagents Hitachi U-2000 ultraviolet spectrophotometer; Shengxue capsule provided by Shanxi Tai Lin Pharmaceutical Co. Ltd. (No. 971101971102971103); the control medicine provided by Chinese: Atractylodes for the control of pharmaceutical and biological products; control products: ammonium ferrous sulfate for four Shanghai reagent factory product, content of less than 99.5% (according to China Pharmacopoeia 1995 two sulfuric acid ferrous under calibration, the result is 98.80%); pH4.2 acetate buffer solution (sodium acetate prepa