白酒混标和内标的做法（Mixed liquor standard and internal standard）.docVIP

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白酒混标和内标的做法（Mixed liquor standard and internal standard）.doc

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白酒混标和内标的做法（Mixed liquor standard and internal standard）

白酒混标和内标的做法（Mixed liquor standard and internal standard） Gas chromatographic analysis of liquor Release time: 2010-09-03 hits: 21 article source: The aroma components of liquor are complex. Besides alcohol and water, there are a lot of aromatic components in liquor. The quality and style of liquor consist of the kinds of aroma components contained in wine and the quantity ratio. The content of alcohols, esters, organic acids, carbon compounds, phenols and high boiling compounds in liquor can be determined rapidly and accurately by gas chromatography. 1. Determination of alcohols, esters and other components in liquor by DNP column (1) determination of main alcohols and esters in liquor by DNP column direct injection method; Alcohols and esters are the main aroma components in spirits. The advantages of the utility model are that the operation is simple, the measurement result is accurate and fast, and the disadvantage is that the extremely micro component is not easy to be detected. 1 Preparation of sample 2% preparation of internal standard: Absorb 2mLs internal standard - n-butyl acetate in the capacity bottle of 1OOmL. (because the internal standard substance is volatile, a small amount of alcohol can be placed in the bottle), and the alcohol content of 55%-60% is constant. The preparation of 1-2% standard samples: We took the acetaldehyde, methanol, propanol, butanol, acetal, butanol, isoamyl alcohol, (hexanol), lmL (furfural), ethyl acetate, ethyl butyrate, ethyl valerate, ethyl lactate, ethyl caproate, isoamyl acetate) of each 2mL to join 1OOmL volumetric flask, 55%-60% (V/V) volume of ethanol, after mixing the sample composition. (add a little ethanol to the volume bottle to prevent evaporation) Mix up the mixture: The standard samples lOmL and internal standard 5mL were extracted with pipette, and 55%-60% (V/V) ethanol was allowed to be 1OOmL. Formulas for calculating I and internal standard contents of components in mixtures: Mi=ci x Vi * di * lO00 Ms=cs x V