尖晶石MgFe2O4纳米粉的水热反萃合成.PDFVIP

98 / 2008 10 MgFe O 2 4 Synthesis of Spinel MgFe O Nano-pow der 2 4 by Hydrothermal Stripping , 珺圆, 王 静, 杨桂琴 ( , 3000 2) WANG Xing-yao, HAN Jun-yuan, WANG Jing, YANG Gu-i qin ( Chemistry Department of T ianjin University, T ianjin 3000 2, China) : ) ) ) , 12~ 18nm M g- Fe O XRD TEM , pH : 2 4 190~ 210 e , MgFe O , 2 4 : ; MgFe O ; ; 2 4 : O61114 : A : 1001-4381(2008) 10-0098-03 2 4 Abstract: A new method of synthesis of spinel MgFe O nano-pow der, the hydrothermal stripping, w as introduced, and it w as applied to synthesize MgFe2 O4 nano-pow ders of 12- 18nm. Some factors in- fluencing morphology and size of MgFe2 O4 powders, such as stripping temperature, the pH and ingre- dients of w ater phase, w ere investigated w ith the help of XRD and T EM . T he results suggest that the MgFe2 O4 nano-pow ders can be synthesized w ith water directly from the mix inorganic phase of iron- loaded and magnesium loaded at 210-220 e . This method can give a typical spinelferrite w ith w ell crystallized, much narrow er particle size distribution shaped in quas-i sphere and w ithout agglomera- tion. Key words: hydrothermal stripping; MgFe2 O4; nano-pow der; synthesis MgFe2 O4 , [ 1] ; ( 3) , , , MgFe2 O4 n , [ 2, 3] , Mg- 2 4 Fe O , [ 10- 15] , - [ 3- 8] , MgFe2 O4