卷烟及烟气中薄荷醇的毛细管气相色谱分析-烟草科技.PDFVIP

32 ★　TobaccoScience Technology★　　　　★　TobaccoChem istry ★　　　　2007 4( 237) 　　　　　 　, 　, 　, , , 　 武汉烟草(集团)有限公司技术中心,武汉市汉阳区十升路 22 号　430051 :毛细管气相色谱;卷烟;滤嘴;烟气; 荷醇 :建立了一种以无水乙醇为提取剂, 茴香脑为内标, 采用毛细管气相色谱定量测定卷烟烟 丝和烟气中 荷醇的方法,并采用该法测定了 6种 荷型卷烟嘴棒、烟丝、烟气粒相物和烟蒂 中的 荷醇含量。结果表明:①该法检测限为 3. 54 ～7. 96ng 支/ , 回收率在 98. 8%～101. 8% 之间, RSD4%;②该法的测定结果与比色法没有明显差异;③剑桥滤片可以完全截留主流烟 气中的 荷醇;④用进入主流烟气中的 荷醇量表征 荷型卷烟的凉度大小, 能更准确地反映 荷型卷烟的感官特征。 :S264. 3　:A　:1002 -0861(2007 )04 - 0032 - 05 Determ ination ofMenthol in Cigarette and its Smokeby Capillary GasChromatography HUANG LONG, CHEN Y,I LIU HU,I LUO CHENG-HAO, SONG XU-YAN, and LIDAN echnology Center ofW uhan obacco (Group)Co., Ltd;Wuhan 430051, China Key ords:Capillary gas chromatography;C igarette;Filter;Smoke;M enthol Abstract:U sing ethanol as a solvent and anethole as an internal standard, amethod for determ ining menthol in cigarette and its smoke by capillary gas chromatography was established. he menthol in cut tobacco, filter, total particulatematter and buttof six brandsofmentholated cigaretteswas dete-r mined by the method and comparedw ith the resultsobtained by UV-V ismethod. he results showed that:1)the detection lmi its reached 3. 54 - 7. 96ng /cig., the recovery ofm entholwas from 98. 8% to 101. 8%, and RSD was below 4%;2)there wasno obviousdifference bewt eenmenthol contents determ ined by capillary gas chrom atography and UV-V is;3)the menthol in mainstream cigarette smoke could be completely trapped by Cambridge filter pad;and 4 )the sensory characteristic of mentholated cigarette could be reflected more exactly by the coolness characterized w ith menthol content in mainstream cigarette smoke. 　　、、 。, [1-2] [3] [1, 4-10] 、 、 [11] 。[4-10],