表面处理剂对聚吡咯·铁氧体复合材料性能的影响.pdfVIP

Advances in Material Chemistry 材料化学前沿, 2017, 5(2), 25-30 Published Online April 2017 in Hans. /journal/amc /10.12677/amc.2017.52003 Effect of the Surface Treatment Agent on PPY/Sr-Ferrite Composites Cunrui Zhang, Rui Zhang, Weifu Zhao, Xiaoming Wang, Guien Zhang No. 33 Research Institute of China Electronics Technology Group Corporation, Taiyuan Shanxi th th th Received: Mar. 24 , 2017; accepted: Apr. 7 , 2017; published: Apr. 12 , 2017 Abstract The M-type Sr-ferrite powders were prepared by using sol-gel method. Powder samples were prepared at 850˚C and different holding time. The phase, size and magnetic properties of the powder samples were characterized by using XRD, SEM and network analyzer. The result indicates that the products that were prepared at 850˚Cand 2 h were pure. The ppy/Sr-ferrite composites were obtained by in-situ polymerization method by different treatment agent. By testing the coer- civity, magnetization and conductivity of the composites obtained by different treatment agents, The effect of treatment agent on the ppy/Sr-ferrite composites properties was given a detailed ex- planation. Keywords PPY, Surface Treatment Agent, Hysteresis Loop 表面处理剂对聚吡咯/铁氧体复合材料 性能的影响 张存瑞，张 锐，赵维富，王晓明，张贵恩 中国电子科技集团公司第三十三研究所，山西 太原 收稿日期：2017年3月24 日；录用日期：2017年4月7 日；发布日期：2017年4月12 日 摘 要 以溶胶–凝胶法制备M型锶铁氧体，在850℃的煅烧温度，不同保温时间的条件下制得粉末样品，并对 制备产物的物相、形貌和磁性能利用XRD 、SEM等检测技术进行表征。实验结果证明：在850℃煅烧，2 文章引用: 张存瑞, 张锐, 赵维富, 王晓明, 张贵恩. 表面处理剂对聚吡咯/铁氧体复合材料性能的影响[J]. 材料化学 前沿, 2017, 5(2): 25-30. /10.12677/amc.2017.52003 张存瑞 等 h煅烧时间所得产物都为较纯的锶铁氧体。通过不同的表面处理剂将制得的钡铁氧体在聚吡咯的乳液中 通过乳液聚合的方法合成了聚吡咯/铁氧体复合材料。通过对不同处理剂得到的复合材料的矫顽力、磁化 强度和电导率的检测，得到表面处理剂对复合材料性能的影响规律。