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改性松香脂环基环氧树脂的固化反应特性-林产化学与工业.pdf

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24 Vol.24 Supplement 2004 8 Chemistry and Industry of Forest Products Aug.2004 孔振武, 黄焕, 周浩 ( 中国林业科学研究院林产化学工业研究所, 江苏南京210042) KONG Z W : ;FT- IR ,, DSC 272~ 335 J/ g; ; A : ; ; :T 351. 471; O636. 9 :A : 0253- 2417(2004)S0- 0029- 04 CHARACTERIZAT ION OF CURING REACT ION OF MODIFIED ROSIN BASED ALICYCLIC EPOXY RESIN KONG Zhen- wu, HUANG Huan, ZHOU Hao ( Inst it ute of Chem ical I nd ust ry of Forest Prod ucts, CA F , N anj ing 210042, Chi na) Abstract: The activity of curing reaction of modified rosin based alicyclic epoxy resin with modified methyl hexahydrophthalic anhydride was investigated by thermal analysis and gelatin time determination. The curing process and reaction mechanism of this epoxy resin/ modified liquid anhydride system were studied by qualitative analysis of FT-IR spectrum and quantitative determination of curing degree. It was shown that curing reaction of this kind of epoxy resin with modified liquid anhydride was an exothermic reaction, and the reaction enthalpy determined by DSC method was 272- 335 J/ g. The gelation time of this epoxy resin with modified liquid anhydride was related to the chemical structure and the composition of epoxy resin, curing temperature and accelerator. The reaction process and curing mechanism were basically identical to the curing reaction of bisphenol A epoxy resin with anhydride in the presence of accelerator. Key words: rosin; alicyclic epoxy resin; curing reaction , , , [1~ 3] :2004- 02- 13 : ( 2001BA501A 14) ; () : ( 1965- ) , , , ,, 30 24 20 70, ,