定向凝固FGH96合金动态再结晶行为研究-北京金属学会.DOCVIP

电渣重熔连续定向凝固技术在高温合金上的应用研究 付 锐， 冯 涤， 陈希春， 任 昊 （钢铁研究总院 高温材料研究所，北京 100081）：采用真空/气体保护电渣重熔连续定向凝固（ESR-CDS）技术制备成功了φ10mm和φ110mm的定向凝固FGH96合金。采用XRD测试了定向凝固柱状晶的生长取向结果表明，柱状晶择优生长方向为100晶向通过扫描电镜对由传统ESR 和ESR-CDS 技术制备的FGH96合金铸态组织进行了对比分析，结果表明，传统ESR 枝晶生长方向凌乱，枝晶间区域较大，枝晶间非平衡析出相数量多，尺寸大，而 ESR-CDS FGH96合金的一次枝晶轴平行生长，二次枝晶臂排列紧密互相咬合，枝晶间析出相尺寸较小，枝晶偏析程度低，经高温退火可完全达到成分均匀化；由非金属夹杂物的统计结果可知，ESR-CDS FGH96合金中最大尺寸非金属夹杂物小于μm，夹杂物总量较传统ESR FGH96合金降低50%， FGH96合金非金属夹杂物总量降低70%以上。通过锻造技术可实现ESR-CDS FGH96合金坯锭的锻造开坯过程，获得具有均匀等轴晶组织的饼坯件，晶粒尺寸约40μm。 ：高温合金电渣重熔连续定向凝固技术偏析：TG 文献标识码： A ：esearch on ESR-CDS about Superalloy FU Rui, FENG Di, CHEN Xi-chun, REN Hao (High Temperature Materials Division, Central Iron and Steel Research Institute, Beijing 100081, China) Abstract: Directionally solidified FGH96 superalloy ingot (φ160mm and φ110mm) were successfully produced by electroslag remelting continuous directional solidification (ESR-CDS) technology. The columnar grain grows parallel with the solidification direction along at 100 crystallographic orientation. The cast structure of ESR-CDS FGH 96 alloy ingot and conventional ESR ingot were analysed by SEM respectively. The result showed that compared with the conventional ESR ingot, the ESR-CDS FGH96 alloy ingot has finer pinetree structure, lower element segregation degree. Uniform distribution of elements can be achieved after heat treatment. The size of inclusion in ESR-CDS FGH96 alloy is less than 5.89μm. Compared with ESR technique and PM process, the inclusion volume in ESR-CDS FGH96 alloy ingot decreased up to 50% and 70%, respectively. The cogging process of ESR-CDS FGH96 alloy ingot was successfully completed by isothermal forging technique. The pan billet got fully recrystallized structure (uniform grain size 40μm) after heat treatment. Key words: superalloy, ESR-CDS technology, dendritic segregation，recrystallization 涡轮盘是航空发动机的关键热端零部件[1]。由于涡轮盘在高温工作环境下承受高的载荷，且本身在高速旋转的同时还起到传送扭矩的作用，工作条件非常苛刻，对材料性能的要求极高。目前制备高合金化航空发动机涡轮盘的工艺主要有两种[1]，一是传统的铸/锻工艺（Cast/Wrought，C/W