直接测汞仪测定食品中总汞含量及结果分析.pdfVIP

Hans Journal of Food and Nutrition Science 食品与营养科学, 2017, 6(3), 181-187 Published Online August 2017 in Hans. /journal/hjfns /10.12677/hjfns.2017.63022 Determination of Total Mercury in Food by Direct Mercury Analyzer * Lei Feng, Chaowen Pu , Heng Li, Renping Zhang Center for Disease Control and Prevention of Fuling District of Chongqing, Chongqing th th th Received: Aug. 6 , 2017; accepted: Aug. 18 , 2017; published: Aug. 28 , 2017 Abstract Objective: To establish rapid determination of total mercury in solid and liquid forms of food, an elemental mercury analyzer (DMA-80) was applied in 9 kinds of food, including grains, meats, ed- ible fungus, eggs, salts, vegetables, milk and dairy products, mineral water, canned food for infants, the analytical results were compared to the commonly used national standard method atomic flu- orescence spectroscopy. Methods: Samples did not need special pretreatment and can be used by direct mercury analyzer to determine the total mercury. Results: According to the experimental conditions, the total mercury was determined by direct mercury analyzer, the sample decomposi- tion time was 2 min, the decomposition temperature of grain and other plant foods was 650˚C, and the decomposition temperature of meat was 850˚C. A linearity was obtained over the range of 0.0- 20.0 ng under the optimum conditions, y = −0+ 0 −02, the cor- relation coefficient was greater than 0.999, recovery rate was 91.0%-102.9%, the relative stan- dard deviation of the determination results was 1.36%-2.87%, and the detection limit was 0.4 μg/kg. Conclusions: There was no statistically significant