硫酸二乙酯提纯装置的改进与智能化研究.pdfVIP

Instrumentation and Equipments 仪器与设备, 2015, 3(4), 129-134 Published Online December 2015 in Hans. /journal/iae /10.12677/iae.2015.34019 Research on Improvement and Intelligent for Purification Device of Diethyl Sulfate Jin Ai, Jianjun Li, Chuande Zhao, Yijian Luo, Qian Zhang, Jie Chen* Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang Sichuan th th th Received: Nov. 25 , 2015; accepted: Dec. 13 , 2015; published: Dec. 16 , 2015 Copyright © 2015 by authors and Hans Publishers Inc. This work is licensed under the Creative Commons Attribution International License (CC BY). /licenses/by/4.0/ Abstract A high effective and intelligent purification device was developed by improving and optimizing the vacuum distillation apparatus of diethyl sulfate. The characterization results of the purified prod- uct showed that the qualified product could be obtained by only once rectification process through the modified vacuum rectification device, which could precisely control the temperature, vacuum degree and split ratio. This modified device has the advantages of simple process and easy opera- tion, as well as intelligent control, which further improve the occupational health and safety. Keywords Diethyl Sulfate, Vacuum Rectification, Purification Device, Improvement, Intellectualization 硫酸二乙酯提纯装置的改进与智能化研究 艾 进，李建军，赵川德，罗毅坚，张 倩，陈 捷* 中国工程物理研究院化工材料研究所，四川 绵阳 收稿日期：2015年11月25 日；录用日期：2015年12月13 日；发布日期：2015年12月16 日 摘 要 本文通过对硫酸二乙酯减压蒸馏装置的改进优化，建立了一套高效智能的提纯装置。提纯产品理化检测 *通讯作者。 文章引用: 艾进, 李建军, 赵川德, 罗毅坚, 张倩, 陈捷. 硫酸二乙酯提纯装置的改进与智能化研究[J]. 仪器与设备, 2015, 3(4): 129-134. /10.12677/iae.2015.34019 艾进 等 结果表明：采用改进后的减压精馏装置进行硫酸二乙酯提纯试验，可以准确控制所需的温度、真空度和 分流比，仅需精馏一次即可