SEM 和EPMA 更深入的课题.pptVIP

SEM and EPMA Some Advanced Topics Beyond the Basics Stereo SEM Example: porous sandstone Stereo SEM Details EDS of particles Particles - 1 Mass effect/error: electrons escape from sides of small particles if E0 is large enough, so quantitative analysis will be in error because different elements (with different binding energies) will be affected differently Particles - 2 Absorption effect of non-flat upper surface: different path length from normal flat geometry and the “normal” way we do quantitative analysis is to use FLAT polished standards for calibration -- so we could have “too much