水热法合成MoO_3纳米带对其光吸收特性的影响.pdfVIP

Rare Metal Materials and Engineering Volume 41, Suppl. 2, September 2012 Cite this article as: Rare Metal Materials and Engineering, 2012, 41(S2): 488-491. The Influence of the Morphologies of MoO Nanobelts 3 Synthesized Using the Hydrothermal Method on Their Optical Absorption Properties Fu Xiaoming Suqian College, Suqian 223800, China Abstract: Crystalline MoO nanobelts of less than 100 nm in radial size have been successfully synthesized with ammonium molyb- 3 date as molybdenum source and nitric acid as precipitant at 240 °C with pH=3 for 96 h by the hydrothermal method. The morpholo- gies and structures of MoO3 have been characterized and analyzed by XRD, SEM, TEM and SAED. SEM confirms that the slender- ness ratio of MoO3 is enlarged with the increase of the reaction temperature and the pH value. SAED analysis shows that the crystal morphology of the synthesized MoO3 nanobelts is crystalline. UV-VIS (Ultraviolet-visible spectroscopy) results show that as synthe- sized MoO3 nanobelts have the good optical absorption property. Key words: ammonium molybdate; hydrothermal method; MoO3 nanobelts; optical absorption property In the past decade, much attention has been focused on one thermal reaction[13], MoO nanoparticles by hot-wire chemical 3 dimensional nanomaterials with different morphologies in- vapor deposition[14], tremella-like MoO2 by the hydrothermal cluding nanotubes, nanowires/nanorods and nanobelts. Be- reduction[15], the fissile MoO by the hydrothermal reaction[16],