聚烯烃塑料溶剂提取物影响因素研究-食品安全质量检测学报.pdfVIP

8 2 Vol. 8 No. 2 2017 2 Journal of Food Safety and Quality Feb. , 2017 1* 2 2 商贵芹 , 尹大伟 , 杨心洁 (1. , 213000; 2. , 213000) 摘 要: 目的 方法 , 结果 / 1 g/100 mL8 () 2 h结论 , 关键词: ; ; ; ; Influencing factors of solvent extracts of polyolefin plastic 1* 2 2 SHANG Gui-Qin , YIN Da-Wei , YANG Xin-Jie (1. Changzhou Entry-Exit Inspection and Quarantine Bureau, Changzhou 213000, China; 2. Changzhou Safety Testing Center for Entry-Exit Industrial and Consumable Products, Changzhou 213000, China) ABSTRACT: Objective To investigate and establish the best method for the determination of the polyolefin resin xylene and n-hexane solvent extracts. Methods The best experimental program was obtained by investigating the effects of the ratio of samples’ mass to solvent volume, filtering method, sample particle size, evaporative drying method, residue drying method and drying time on n-hexane and xylene solvent extracts of polyolefin resin. Results The optimal experimental conditions were as follows: the ratio of samples’ mass to solvent volume was 1 g/100 mL, the sample particle size was less than 8 mesh holes (sample particle size of xylene extract could not be limited), xylene solvent extract could not add antiox