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Surfactant-Assisted Solvothermal Synthesis of CeO Hollow
2
Nanospheres
Zhijie Yang, Hui Liang, Ling Liu, Hongxiao Yang, Yanzhao Yang1
School of Chemistry and Chemical Engineering, Shandong University 250100, People’s Republic of
China
Abstract
CeO2 hollow nanospheres were synthesized via a facile surfactant-assisted solvothermal route.
The synthesized products were characterized by X-ray diffraction (XRD), field emission scanning
electron microscopy (FESEM), transmission electron microscopy (TEM), selected area electron
diffraction (SAED) and N2 adsorption-desorption. TEM results indicated that these hollow spheres
had average diameters of ca. 150 nm. N2 adsorption-desorption showed that the specific surface area
2
of the nanospheres was 83.2 m /g. The possible formation mechanism of CeO hollow nanospheres
2
has also been proposed.
Keywords: CeO2 ; Solvothermal; Nanomaterials; Porosity
1. Introduction
Transition metal oxide hollow structures have attracted great investigative interests due to their
various applications in catalysts, microreacters, drug delivery, chemical sensors, biotechnology, and
so on [1, 2]. So far, numerous methods have been developed to synthesize hollow structures of many
materials, including template-assisted synthesis, and the Kirkendall effect, among which the
template-assisted method is the most universally adopted for the preparation of hollow structures.
One straightforward approach to hollow structures is based on coating hard templates with the
desired
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