CHM 152LL The Solubility Product of Calcium Hydroxide：CHM 152ll氢氧化钙溶度积.docVIP

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CHM 152LL The Solubility Product of Calcium Hydroxide：CHM 152ll氢氧化钙溶度积.doc

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CHM 152LL The Solubility Product of Calcium Hydroxide：CHM 152ll氢氧化钙溶度积

CHM 152LL: The Solubility Product of Calcium Hydroxide Introduction: Calcium hydroxide, Ca(OH)2, is considered a slightly soluble substance in water. Ca(OH)2 (s) Ca2+ (aq) + 2OH- (aq) Ksp = [Ca2+][ OH-]2 In this experiment, we will measure and concentration of Ca2+ in a saturated solution of Ca(OH)2 and calculate the Ksp, solubility product constant, for Ca(OH)2. We are going to obtain a saturated solution of Ca(OH)2. Then filter out the solid Ca(OH)2. The [Ca2+] will be obtained through titration with a solution of EDTA4- (ethylenediamine tetraacetate). EDTA4- and Ca2+ react to for the complex ion Ca(EDTA)2-, Ca2+ (aq) + EDTA4- (aq) Ca(EDTA)2-(aq) The indicator Eriochrome Black T (EBT) changes color in the presence of Ca2+. Without Ca2+, it is blue; with Ca2+, it forms a red complex ion. When EDTA4- reacts with all the Ca2+, the indicator EBT looses it Ca2+ and reverts from red back to its original blue. This color change will indicate the endpoint where all the Ca2+ has reacted with the EDTA4-. At this point, we can calculate the moles of EDTA added, the moles of Ca2+ it reacted with, thus [Ca2+], [ OH-] and Ksp. Material: 125 mL beaker 125 mL Erleneyer flask 10_mL pipet EBT indicator solution Saturated Ca(OH)2 solution ___________ M EDTA solution Experimental Procedure 1. Pour 50 mL of saturated Ca(OH)2 solution into a 125 mL beaker. Do not shake up the solution bottle. It is saturated and there is solid on the bottom. 2. Filter your Ca(OH)2 solution into a dry 125 mL Erlenmeyer flask. 3. Obtain a 30 mL (or 50 mL) beaker to be used to cover up the Erlenmeyer flask when it is not in use. 4. Measure the temperature of the solution in the Erlenmeyer flask with a clean, dry thermometer. 5. Rinse a clean burette with 5 mL portions of EDTA solution. 6. Fill the burette with the EDTA solution. 7. Pipet 10 mL of the filtered Ca(OH)2 solution into another clean 125 mL Erlenmeyer flask. Add 2 drops of EBT indicator. 8. Titrate the Ca(OH)2 solution with the EDT