本科毕业论文-蔗糖酯合成研究.docVIP

蔗糖酯的合成研究 摘要 本文综述了蔗糖酯的合成方法及工艺的研究进展,并对其反应机理进行了阐述。包括蔗糖酯的合成工艺、纯化检测方法、工业用途和开发现状 ,最后还提出了蔗糖酯的研究开发设想本法以和蔗糖为原料,一步反应合成脂肪酸蔗糖酯。反应产物可按所需的HLB值进行精制和分离,同时尚可副产单脂肪酸甘油酯。The Study of Synthesis of Sucrose Esters Abstract This paper reviews the synthesis and procedure of sucrose esters, also presents its reaction mechanism. Such as synthetic method, method of purification and determination, industrial application and development situation. This paper also puts forward some research and development ideas of sucrose ester.There are mainly four ways to synthesize sucrose esters: solvent method, emulsification method, homogeneous non-solvent method and enzyme catalyst method. Sucrose esters (SE) are a kind of new type high efficiency emulsifier and surfactant. It has a wide use in industries. The development at home and abroad and the use in industries of SE are reviewed in the paper. This process relates to a sucrose esters prepared by the derect reaction of sucrose with fatty acid methyl ester used as the raw material. The crude product can be purificated by desirable HLB valne; and monoglyceride of the fatty acid is obtained as by-product in the purification. In this experiment, we use sucrose and fatty acid methyl ester as reactant, K2CO3 as catalyst, Glycerol and acetone as co-melting solvent, under the conditions of homogeneous liquation, the reaction of ester exchange is completed. The reaction product is sucrose ester. The best reaction condition is : the ratio of sucrose and fatty acid methyl ester(weight ratio)=1:2,catalyst is 6%, 6 reaction temperature is 120℃,reaction time is 3h,reaction pressure ≤690Pa. Productivity is 45%. For synthesis we use ethyl acetate as extraction. Separate at high temperature, the ethyl acetate can be separated with glycerol. We can do this several times in order to raise the rate of refinement. Keywords：Sucrose esters; synthesis; purification 目录 1 文献综述 1 1.1 概述 1 1.2 蔗糖酯的性质 2 1.3 蔗糖酯的应用 3 1.3.1 食品行业 4 1.3.2 日用化工 8 1.3.3 医药行业 8 1.3.4