开桶即用氮化铝陶瓷金属化专用钨粉的开发.真空电子技术,2015.PDFVIP

·氮化铝技术的发展· “开桶即用氮化铝陶瓷金属化专用钨粉的开发 周增林，惠志林，李艳，林晨光 (北京有色金属研究总院粉末冶金及特种材料研究所，北京100088) of PowdersAvailableforAluminum Tungsten Development Nitride without MetallizingGrinding ZHOU Zhi—lin，LIYan，LIN Zeng—lin，HUI Chen—guang and MaterialsResearch ResearchInstitute (PowderMetallurgySpecial Department，Generalfor Nonferrous 100088，China) Metals，Beijing nitrideceramics without different availableforaluminum Abstract：Fivetungstenpowders metallizinggrinding weremanufacturedthe ammonium re— by including process distil— ductionandadvanced sizeofmanufactured a normal dispersion．Theparticle tungstenpowderpresentsgood with— butionduetothehollowthin-wall structureofthemodifiedAPT．The available spherical tungstenpowders out canincreasethe ofaluminumnitrideceramics grinding quality metallizing． metallizing， Keywords：Tungstenpowder，Aluminumnitride，HightemperatureCO—firing，Ceramic Availablewithout grinding 摘要：本文采用钨酸铵改性一热解一氢气还原一精细加工的工艺，制备了“开桶即用”氮化铝(AIN)陶瓷金属化专用钨粉。 改性钨酸铵的颗粒形貌为空心薄壁球形，该结构保证了钨粉的粒度分布呈现良好的正态分布；通过适当的工艺调控，可稳定 获得五种不同规格的专用钨粉。专用钨粉的开发有助于实现A1N陶瓷的金属化并能提高产品质量。 关键词：钨粉；氮化铝；高温共烧；陶瓷金属化；开桶即用 中圈分类号：TFl22文献标识码：A 文章编号：1002--8935(2015)0