微波消解_ICP_MS法测定土壤_沉积物中多元素_刘翠梅.pdfVIP

( ) 30 1 Journal of Capital Normal University No. 1 2009 2 (Natural Science Edition) Feb. , 2009 - ICP- MS * ** ( , 100037) - (ICP- MS) 12 . , 3 mL HNO - 1 ml HCl- 1 mL HF .5 3 , . 0101~ 3164 ng#g- 1 RSD 3164% . : , ICP-MS, , , . : O 657163 1 , 111 , Agilent 7500c . , . : ; : , Piltier ( 2? 011) e ; : , 215 mm [ 1] . ; : Pt . HNO3 - HF - Mill-i Q (Millipore, Bedford MA) . H2 SO4 HNO3 - HCl- HF- HClO4 [ 2, 3] . 112 , ; : 10 LgPmL VCrCoNiCuZn , . AsMoCdT1PbU , Agilent [ 4] - 1 103 185 HNO - HCl- HF , , . ; : 1010 Lg#mL Rh Re 3 , ; : , Merck [ 5] . ; : BV-III , ; :MOS , ; ICP-MS , - 1 : 10 ng#mL LiCoYCeT 1 . , Agilent ; : 1812M8 , Milli-Q - , . VCrCoNiCu ( GBW07403, GBW07405, ZnAsMoCdT1PbU , GBW07407, GBW08303 ) , . ( GBW08301) . 113 : 2008-01-25 - 1