纤维织物复合材料组分材料体分比的显微CT试验.docVIP

纤维织物复合材料组分材料体分比的显微CT实验测定法 王浩，王 （国防科学技术大学，湖南 长沙 410073） 摘要： 关键词： 中图分类号：TB332 文献标志码：　　　文章编号： Measurements of volume fractions of component material of textile composite using Micro CT experiments WANG Hao, WANG Zhongwei (Science and Technology on Scramjet Laboratory, National University of Defense Technology, Changsha 410073, China) Abstract: A method of measuring volume fractions of component material of textile composite by using Micro CT experiments is developed in this paper. This method can present global, local fiber and yarn volume fractions by Micro CT images in different scales, which can also offer solutions to the difficult volume fractions measurement of component materials of some composites which cannot be measured directly by conventional physical experiments. An E-Glass/Epoxy textile composite was used to illustrate the feasibility and reasonability of the method by the comparisons of the measured values among ASTM D3171 Procedure G, SEM and Micro CT experiments. Corresponding image processing methods to SEM and Micro CT images were used to acquire the accurate component material segmentations. The measurement of Micro CT experiments can be widely applied to measure the volume fractions of component materials of composite. Keywords: E-Glass/Epoxy; Textile composite; Volume fraction; Micro CT; SEM; Image segmentation  近年来，Micro Computed Tomography (显微CT)技术已经成为研究复合材料微观结构的一种重要手段。Desplentere等[1]通过比较4种不同3D编织复合材料的纤维束厚度、宽度及间距参数在表面扫描照片、光学显微照片和显微CT图像中的测量值，说明了编织复合材料显微CT图像反映微观结构的可靠性。Madra等[2]利用显微CT技术对织物复合材料中的孔隙分布进行了多尺度分析。Pazmino等[3]利用显微CT技术研究了面内剪切变形对三维正交编织复合材料纤维束几何参数的影响。Schell等[4]利用显微CT技术对纤维织物复合材料中的纤维束几何形状和孔隙进行了量化研究。一种基于显微CT图像的典型统计方法用于研究织物复合材料纤维束的微观结构特征[5],[6]。王浩等[7]利用高分辨率显微CT技术研究了C/Epoxy织物复合材料纤维束特征参数的统计特征。 在织物复合材料的力学计算模型[8]-[12]中，纤维束在复合材料中的体积分数（简称纤维束体分比）和纤维在纤维束中的体积分数（简称局部纤维体分比）是两个重要的参数。这两个参数虽然可以通过理论计算[13]-[16]近似得到，但真实建模中需要精确测量这两个参数来消除误差。通常情况下，通过物理实验（如ASTM D3171 Procedure G[17]（简称D3171 G实验）或化学消蚀法）只能测得纤维在材料中的体积分数（简称全局纤维体分比），无法直接测得局部纤维体分比和纤维束体分比。此外，对于C/SiC等陶瓷