钒酸铋%2f氮化碳复合材料的制备及其光催化性能的研究.pdf

ABSTRACT Because the graphite carbon nitride in the photocatalytic degradation of pollutants, to visible light absorption ability is weak, through the experiment in this paper, with C N and BiVO compound, preparation of new 3 4 4 photocatalytic materials BiVO /g-C N . By ultraviolet-visible diffuse 4 3 4 reflection (UV-Vis/DRS), X-ray powder diffraction (XRD),scanning electron microscope (SEM), infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS), transmission electron microscope (TEM),and other means of testing, Separately on the BiVO ,C N , BiVO /g-C N structure, elemental 4 3 4 4 3 4 composition, particle shape and absorption of visible light range were characterized. Follow-up was studied by a series of experiments in detail in the visible(400 nm λ 780 nm) with BiVO /g-C N photocatalyst to 4 3 4 photocatalytic degradation of organic pollutants Rhodamine B, through the experimental results, determine the optimum synthesis conditions of catalysts, load ratio and the dosage and the initial concentration of reaction system pH value, solution conditions. By ultrasonic method in the visible light (400 nm λ 780 nm) under the catalytic activity of active C N and BiVO composites BiVO /g-C N . In its 3 4 4 4 3 4 characterization results has proved that the existen