毕业设计（论文）-FeCoNiCrAl高熵合金的组织特征和力学性能研究汇.docVIP

摘 要 本文利用真空电磁感应定向凝固装置分别研究了体积凝固状态下和定向凝固条件下FeCoNiCrAl高熵合金的组织特征和力学性能。研究结果表明: 体积凝固条件下FeCoNiCrAl合金具有简单的BCC结构FeCoNiCrAl高熵合金铸态组织为树枝晶FeCoNiCrAl高熵合金在定向凝固过程中，随着抽拉速度的增大，凝固界面发生平-胞-枝转变胞晶数目增多，胞晶间距减小平界面凝固的稳定性判据枝晶间的显微硬度比的硬度大，原子容易在枝晶间发生偏析，而且原子的体积相对其他原子较大，造成晶格的畸变较大定向凝固区域的硬度小于淬火区的硬度FeCoNiCrAl合金Abstract In this paper, Microstructure and mechanical properties of FeCoNiCrAl high-entropy alloy were investigated under the bulk solidification and directional solidification respectively. The results show that the as-cast microstructure of FeCoNiCrAl high-entropy alloy have simple BCC structure. Typical dendritic structures are observed in the alloy. During the directional solidification, the planar-cellular-dendritic transition of solidification interface can be found with increasing growth velocity. Meanwhile, the number of cellular increases but cellular spacing decreases. Stability criterion of plannar to celluar interface is employed to analyse the interface morphology of directionaly solidified FeCoNiCrAl high-entropy alloy. Experimental investigation was carried out on the microhardness of FeCoNiCrAl alloy under the both bulk solidification and directional solidification condition. The interdendritic microhardness is larger than the one in the first dendritic, because Cr atoms are rich in the interdentrictic segregation, and atom radius of Cr is larger than that of other elements, distortion of crystal lattice is more severe, and microhardness in the directional solidification zone is smaller than the one in the as-quenched due to little distortion of crystal lattice during directional solidification. Keywords: FeCoNiCrAl alloy;directional solidification; interface morphology; microhardness 目录 摘要 I Abstract II 第1章 绪论 1 1.1 课题背景 1 1.2 定向凝固技术发展与研究现状 2 1.2.1 定向凝固技术的发展与应用 2 1.2.2 定向凝固理论研究现状 7 1.3 多主元高熵合金研究现状及发展前景 9 1.3.1 多主元高熵合金研究现状 9 1.3.2 多主元高熵合金的发展前景 17 1.4 本论文研究的主要内容 18 19 2.1 研究方案 19 2.2 实验设备 19 2.3 实验方法 21 2.3.1实验合金及金相试样的制备 21 2.3.2温度采集系统 22 2.3.3定向凝固过程 25 2.4显微组织分析 25 3章 FeCoNi