改良的酸—碱两步法纯钛表面生物活化-improved acid-base two-step method for biological activation of pure titanium surface.docxVIP

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2018-05-29 发布于上海
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改良的酸—碱两步法纯钛表面生物活化-improved acid-base two-step method for biological activation of pure titanium surface.docx

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改良的酸—碱两步法纯钛表面生物活化-improved acid-base two-step method for biological activation of pure titanium surface

AbstractThetexttreatedthesurfaceofTithroughimprovedacid-alkalitwostepsapproach.ResultofSBFsoakingwasregardedasevaluationlevelofTisurfacebioactivity.Thetextstudiedtechnologicalparametertoeffectruleofbioactivity.Phaseconstituent、roughstate、surfacemorphologyandsurfacecontentwerefullyshownbyanalysistestmethodofXRD、AFM、SEMandEDS.Aftersoaking,bondingstrengthbetweenCa-PcoatingandTimatrixwastestedbydirecttensionmethod.Comprehensionofbioactivityandbondingstrengthfinallydeterminedthebestbioactivationtechnology.Improvedacid-alkalitwostepsapproachtechnologydividedacidtreatmentandalkaliheattreatment.Thebestacidtreatmenttechnologywasmixingsolutionof18%HCland3%HFasvolumeratio3:1.Thebestmixingalkaliheattreatmenttechnologywasmixingsolutionof5mol/LNaOHand0.02mol/LCa(OH)2at90℃for24hoursandfollowingat600℃andholdingtimefor1h.Improvedacid-alkalitwostepsapproachtechnologyshortenedtheCa-Pcoatingformingtime.ResultofSBFsoakingat37℃showedthatsurfaceformedHAcoatingassoaking1day.Coatingwasintegrated.Grainswerefineanduniform.Ca/Pwas1.61nearto1.67ofhumanbone.TheresultofdirecttensionshowedthatbondingstrengthbetweenCa-PcoatingandTimatrixwas23.35～25.42MPa.AfterTiwastreatedbyimprovedacid-alkalitwostepsapproach,Tisurfacewasnetporousstructure.PhasesofsurfacemainlywereRutile、CaTiO3andafewAnatase.TisamplesofactivationtreatmentweresoakedinSBF.SurfacegeneratedhydrolyzationreactionandproducedTi-OHbasegroupofnegativeelectrification.Atthesametime,Ca2+ironswerereleased.HydrolyzationreactionimprovedOH-amoutandnegativeelectricityandmadesolubilityproductofCa2+,PO43-andOH-increaseandreachacertainsupersature.Itprovidedadvantagesituationfornuclei.KeywordsBioactivity;surfacemodification;puretitanium;acid-alkaliheattreatment;bondingstrength目录摘要...............................................................................................................................IAbstract.......................................................................................................................II第1章绪论.................