高q中介catio3-lnalo3ln=nd、la系微波介质陶瓷的研究-study on cati o3 - lna lo 3 ln = nd, la microwave dielectric ceramics with high q medium.docxVIP

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高q中介catio3-lnalo3ln=nd、la系微波介质陶瓷的研究-study on cati o3 - lna lo 3 ln = nd, la microwave dielectric ceramics with high q medium.docx

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高q中介catio3-lnalo3ln=nd、la系微波介质陶瓷的研究-study on cati o3 - lna lo 3 ln = nd, la microwave dielectric ceramics with high q medium

AbstractCombined with the development of modern communications technology and microelectronics technology, as a theoretical support for the research status and achievements of high-Q intermediary microwave dielectric ceramics both at domestic andabroad, CaTiO3-LnAlO3(Ln=Nd、La) ceramics are chosen as research system in thisdissertation. The relationships between the component formulations, process of preparation, microstructure and microwave dielectric properties of samples were discussed in detail by using X-ray diffraction (XRD), scanning electron microscopy (SEM) and parallel plate test system.0.7CaTiO3-0.3（LaxNd1-x）AlO3 solid solution was prepared by using La3+ to substitutethe Nd2+ of the CaTiO3-LaAlO3 ceramics. It is found that εr and τf increase as the increase of the x value. The 0.7CaTiO3-0.3(LaxNd1-x)AlO3 ceramics get the max Q×f value, when x=0.5, which may be caused by the ion ordering of the ceramics. As the increase of the sintering temperature, εr and Q×f value increase firstly and then have the trend of decrease. Theoptimal sintering temperature is 1550℃.To adjust the microwave dielectric properties of the 0.7CaTiO3-0.3(La0.5Nd0.5)AlO3 ceramics, moderate amount of SrTiO3 was added into the samples. By adding small amount of SrTiO3, the Q×f value increases as the increase of the density. As the content of SrTiO3 increases, the Q×f value has the trend of decrease and the optimal addition content of SrTiO3 is 0.01 at.%. Because of small low volume fraction of SrTiO3, it has little effect on εr of samples. The change of the τf value is complicated, which needs future investigate. As the increase of the sintering temperature, εr and Q×f value increase firstly and then have thetrend of decrease, and the optimal sintering temperature is 1550 ℃.To explore the effect of Ga2O3 which was added to the samples, 0.7CaTiO3-0.3(La0.5Nd0.5)(Al0.5Ga0.5)O3 was prepared by using 50 at.% Ga3+ to replace Al3+.The results shows that the Ga3+ amount to 50 at.% which was