gdnp共掺杂对tio2sio2nife2o4磁载纳米复合光催化剂性能的影响-effect of gdnp codoped on the performance of tio _ 2 sio _ 2 nife _ 2 o _ 4 magnetically supported nano-composite photocatalyst.docx

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gdnp共掺杂对tio2sio2nife2o4磁载纳米复合光催化剂性能的影响-effect of gdnp codoped on the performance of tio _ 2 sio _ 2 nife _ 2 o _ 4 magnetically supported nano-composite photocatalyst.docx

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gdnp共掺杂对tio2sio2nife2o4磁载纳米复合光催化剂性能的影响-effect of gdnp codoped on the performance of tio _ 2 sio _ 2 nife _ 2 o _ 4 magnetically supported nano-composite photocatalyst

2.3.2 光催化剂的表征 ····································································· 152.3.3 TiO2 纳米复合光催化剂的光活性评价16第 3 章以尿素为氮源溶胶-水热法制备 Gd-N-P-TiO2 纳米光催化剂及其表征 183.1 引言························································································· 183.2 Gd-N-P-TiO2 纳米光催化剂的制备工艺研究183.2.1 Gd-N-P 共掺杂 TiO2 纳米光催化剂的正交实验优化183.2.2 焙烧温度对 Gd-N-P 共掺杂 TiO2 纳米粒子光活性的影响203.3 结果与讨论················································································ 21XRD 分析21TEM 分析22BET 分析22XPS 分析23FT-IR 分析243.3.6 UV-vis 可见吸收光谱分析253.3.7 PL 分析253.3.8 探讨掺杂对 TiO2 光活性的影响及协同机制263.4 本章小结··················································································· 28 第 4 章以氨水为氮源溶胶-水热法制备 Gd-N-P-TiO2 纳米光催化剂及其表征···· 30 4.1 引言························································································· 304.2 结果与讨论················································································ 30XRD 分析30TEM 分析31BET 分析32XPS 分析33FT-IR 分析34UV-vis 吸收光谱分析35PL 分析364.2.8 掺杂对 TiO2 光活性的影响及机制探讨364.3 本章小结··················································································· 39 第 5 章 Gd-N-P 共掺杂对 TiO2/SiO2/NiFe2O4 磁载纳米复合光催化剂性能的影响 40 5.1 引言························································································· 405.2 结果与讨论················································································ 405.2.1 TiO2/SiO2/NiFe2O4 磁载纳米复合光催化剂的制备工艺研究 405.2.2 Gd-N-P 掺杂对 TiO2/SiO2/NiFe2O4 活性及磁性的影响 435.3 本章小结··················································································· 45 结论 ······························································································ 47 参考文献 ··························································································· 49攻读硕士学位期间发表的学术论文·························································· 60哈尔滨师范大学学位论文原创性声明······················································· 61哈尔滨师范大学学位论文版权使用授权书 ················································ 61致谢 ···················································