广西产五月艾挥发油气相色谱-质谱联用分析.docVIP

广西产五月艾挥发油气相色谱-质谱联用分析 　　【摘 要】:目的:分析研究广西产五月艾挥发油的主要化学成分#65377;方法:采用水蒸气蒸馏法提取五月艾挥发油,并通过GC-MS对挥发油成分进行鉴定,用面积归一化法计算其相对百分含量#65377;结果:广西产五月艾挥发油的得率为0.40%,从挥发油中鉴定了62个成分,占总离子流图峰面积的92.71%,其中主要成分为:[1R-(1R*,4Z,9S*)]-4,11,11-三甲基-8-亚甲基-二环[7.2.0]-4-十一碳烯(11.05%)#65380;大根香叶烯D(10.52%)#65380;石竹烯氧化物(7.15%)#65380;龙脑(5.34%)#65380;石竹烯(4.02%)#65380;斯巴醇(3.84%)#65380;桉油精(3.80%)#65380;松油醇(2.29%)等#65377;结论:此方法简便可靠,可为合理使用广西产五月艾药材提供一定的科学依据#65377; 　　【关键词】:广西;五月艾;挥发油;GC-MS 　　【中图分类号】R284.1【文献标识码】 A【文章编号】1007-8517(2009)01-0027-03 　　 　　Analysis of Chemical Constituents of Volatile Oil from Artemisia indica of Guangxi by GC-MS 　　WEI Zhi-ying, WU Huai-en, LIANG hai-yan 　　( Guangxi University of TCM, Nanning Guangxi 530001,China ) 　　AbstractObjective: To analyze the chemical constituents of volatile oil from Artemisia indica Willd. of Guangxi. Methods: The volatile oil was extracted from Artemisia indica Willd. by steam distillation. The components of volatile oil were separated and identified by GC-MS. The relative content of each component was detemined by area normalization. Results: The yield rate of the collected volatile oil of Artemisia indica Willd. was 0.40%, and sixty-five kinds of components were identified, accounting about 92.71% of the total volatile oil. The main constituents of it were as follows: [1R-(1R*,4Z,9S*)]-4,11,11-trimethyl-8-methylene- Bicyclo[7.2.0]undec-4-ene (11.05 %), Germacrene D (10.52 %), Caryophyllene oxide (7.15 %), Borneol (5.34 %), Caryophyllene (4.02 %), Spathulenol (3.84 %), Eucalyptol (3.80 %), Terpineol (2.29 %) etc. Conclusion: It can be provide a scientific basis for fair use of Artemisia indica Willd. of Guangxi. 　　Key wordGuangxi; Artemisia indica Willd.; volatile oil; GC-MS 　　 　　五月艾为菊科植物五月艾Artemisia indica Willd.的干燥地上部分,性微温,味辛#65380;微苦#65377;归脾#65380;肝#65380;肾经#65377;具有祛风消肿,止痛止痒,调经止血之功效,可???于治疗偏头痛,月经不调,崩漏下血,风湿痹痛,疟疾,痛肿,疥癣,皮肤瘙痒等症#65377;与药典收载的艾叶即菊科植物艾Artemisia argyi Levl.et Vant.的干燥叶的性味#65380;功效相似[1,2]#65377;五月艾在广西的野生资源较为丰富,多以其作艾叶入药,《中药大辞典》中也有“……其叶(五月艾)