精馏分离异醚毕业论文.docVIP

毕业论文 题 目 学 院 专 业 班 级 学 生 学 号 指导教师 二〇一 二年六月十日ABSTRACT In this paper,chemical plant samples Boshan waste ether, the main ingredient is isopropyl ether and 1,2 - dichloroethane, by gas chromatography analysis, the raw material in the mass fraction of isopropyl ether was 14.4%, 1,2 - dichloroethanethe mass fraction of 72.9%, the two components no azeotropic batch distillation separation separation. Right the sample Boshan waste ether carried out distillation, analysis of the its the the main componste ether, and enable it to reach re-use the purity of. Experiment to build a batch distillation tower section height of 1.6 meters, diameter of column 26mm, samples were separated by batch distillation experiments, and distillation products were detected by gas chromatography. The results show that the, through the intermittent distillation method can be The samples were separation, can get the a purity of greater than 98% of the 1,2 - dichloroethane products. Distillation means purification conditions of the feasibility of re-use of waste ether, used distillation column in this paper the theoretical plate number of 11. Key words：Isopropyl ether；Separation and purification；Distillation 目 录 摘要……………………………………………………………..…….….…………….. .I ABSTRACT….……………….……….….………….……………………..…………….II 1 前言….…….….………….…………………………………………….….……………..1 1.1 异丙醚的理化性质..……..…….…........................………….………….………..1 1.2 危险性概述............…......….….........……….......…………….………….………..1 1.3 消防措施................…………......…………………………….…....……..………1 1.4 制备......………………………................………………………….…....……….2 2 间歇精馏概述......................……..….………………………….…..….………….3 2.1间歇精馏概论…………………………………………………………………..3 2.2 间歇精馏的影响因素………………………….………………...………………..3 2.2.1 过度馏分的影响……………………………….…………………………...3 2.2.2 回流比的影响………………………………….…………………………...4 2.2.3 温度的影响……………………………… …………… …………………4