镍基纳米材料的控制合及性能研究.docVIP

镍基纳米材料的控制合成及性能研究 摘 要 镍基纳米材料作为纳米材料中的一类重要复合材料，因为其在磁记录、催化剂、光伏电池、抗癌药物磁性载体等领域的广泛应用而成为研究的热点。本研究首先确定了合成镍纳米材料的有效方法和一些影响其合成的因素，然后通过以氢氧化镍为连续相复合其他物质来合成镍基纳米材料，并通过SEMXRD、红外等方法对产物进行表征，同时测试其性能。结果表明所得的材料具有的性能有可能通过进一步研究得以应用。Nickel base nano materials as one of the most important composite materials in nanometer materials, due to its stable chemical properties has extensive application in many ways. Because of its in magnetic recording, catalyst, photovoltaic cells, anti-cancer drugs are widely used in the field of magnetic carrier, etc and become the research hot spot ，This study first determine nanomaterial synthesis nickel effective method and some factors affecting the synthesis, and then studied with nanometer nickel as continuous phase composite material for synthesis of other nickel base the electrochemical properties of nanomaterials. By SEM, XRD, ir and other methods of product have been characterized, at the same time to test its electrochemical performance. Through related characterization of XRD, ir is the experiment of the composite materials of product is the target product. But also detect the electrochemical properties of the composites, the results show that the composite material has good electrochemical properties, may by further research to application. Obtained by the experimental study of the synthesis of nanometer nickel to join in the reaction system of NH4Cl will get internal reticular structure of globular nanometer Ni(OH)2, did not add the ruleless petal shaped product.In Ni(OH)2, respectively, and the polymerization of pyrrole and aniline compound products used to test their electrochemical properties, electrochemical properties of the composites has been increased obviously. By changing or optimize the experimental conditions should be able to continue to improve the performance of the composite material, make it has higher practical value. Keywords: Nickel hydroxide; Pyrrole; Composite materials;application