年产30吨甲醇_毕业设计.doc

东北石油大学本科生毕业设计（论文）PAGE PAGE 33东北石油大学本科生毕业设计（论文）年产30万吨甲醇毕业设计摘 要甲醇是由CO和H2合成的，本设计分析了操作条件：温度、压力、原料气组成、空速和惰性气体对甲醇生产的影响，本设计采用煤为原料，通过GSP气化工艺将原料煤气转化为合成气，通过变换和NHD脱硫脱碳工艺把合成气转化为满足甲醇合成条件的原料气，在列管式等温反应器中合成甲醇，本设计采用XNC-98型催化剂，利用三塔精馏工艺将生成的粗甲醇精制后得到精甲醇。设计的主要内容包括能量衡算和主要设备的选型，能量衡算有物料衡算和热量衡算，主要设备包括甲醇合成塔和精馏塔。 关键词：甲醇；合成；精馏 AbstractMethanol consists of CO and H2，this design analysis the effects of operation conditions: temperature, pressure, the gas material composition, airspeed and inert gas , this design uses the coal as raw material, through the GSP gasification process will raw materials gas into snags, through the transformation and NHD desulfurization process into the decarburization snags methanol synthesis conditions meet gas material, in the tube type of methanol synthesis isothermal reactor, this design uses the XNC-98 type catalyst, use three tower distillation process will create the thick methanol blended get fine methanol. The design of the main contents include energy calculation and major equipment selection, energy balance calculations have material calculation and heat balance calculations, the main equipment including methanol synthesis tower and rectifying tower. Key words：Methanol；Synthesis；Rectification目 录 TOC \o 1-1 \h \z \u \t 标题 2,1 HYPERLINK \l _Toc327893318 第1章 概述 PAGEREF _Toc327893318 \h 1 HYPERLINK \l _Toc327893319 第2章 工艺简介及影响因素 PAGEREF _Toc327893319 \h 2 HYPERLINK \l _Toc327893320 2.1甲醇合成工艺简介 PAGEREF _Toc327893320 \h 2 HYPERLINK \l _Toc327893321 2.2操作条件对反应过程的影响 PAGEREF _Toc327893321 \h 2 HYPERLINK \l _Toc327893322 第3章 甲醇生产工艺流程 PAGEREF _Toc327893322 \h 5 HYPERLINK \l _Toc327893323 3.1甲醇合成工艺流程 PAGEREF _Toc327893323 \h 5 HYPERLINK \l _Toc327893324 3.2 甲醇精馏工艺流程 PAGEREF _Toc327893324 \h 6 HYPERLINK \l _Toc327893325 第4章 工艺计算 PAGEREF _Toc327893325 \h 8 HYPERLINK \l _Toc327893326 4.1物料衡算 PAGEREF _Toc327893326 \h 8 HYPERLINK \l _Toc327893340 4.2能量衡算 PAGEREF _Toc327893340 \h 16 HYPERLINK \l _Toc327893344 第五章 主要设备的计算