气相色谱法分析火灾环境残留物中汽油·煤油·柴油.pdfVIP

Advances in Environmental Protection 环境保护前沿, 2017, 7(4), 359-365 Published Online August 2017 in Hans. /journal/aep /10.12677/aep.2017.74048 Analysis of Gasoline, Kerosene and Diesel Fuel in Fire Environment Residue by Gas Chromatography * Guanglin Song, Xijuan Xu , Diyong Chen, Fei Xiao Guizhou Academy of Testing and Analysis, Guiyang Guizhou rd th th Received: Aug. 3 , 2017; accepted: Aug. 18 , 2017; published: Aug. 28 , 2017 Abstract To determine qualitative and quantitative analysis of gasoline, kerosene and diesel in fire resi- dues, extracting liquid of fire residue was compared with gasoline, kerosene and diesel by gas chromatography analysis, the gasoline, kerosene and diesel determined qualitatively by the re- tention time of the main characteristic peaks. The content of the characteristic components of gasoline, kerosene and diesel was proportional to the size of its peak area. The gasoline, kerosene and diesel were determined quantitatively by the normalization of the characteristic peak area. The minimum detection limit of gasoline, kerosene and diesel, respectively was 100 μL/L, 100 μL/L, 200 μL/L. The regression equation of Sinopec No. 93 gasoline volume concentration and the total value of five characteristics peak area was Y = 0.0458X + 0.602, the correlation coefficient was 1. The regression equation of Sinopec kerosene volume concentration and the total value of four characteristics peak area was Y = 0.0419X −2.2658, the correlation coefficient was 0.9999. The regression equation of Sinopec No. 0 diesel fuel volum