年产6800吨醋酐装置工艺设计.docVIP

PAGE PAGE PAGE 27 吉林化工学院 成人教育学院毕业设计 6800吨/年醋酐装置精馏工段工艺设计 学生学号 学生姓名 专业班级 111 化学工程与工艺 指导教师 丁 斌 教 授 完成日期 2011.09.03 吉林化工学院 Jilin Institute of Chemical Technology  摘 要 本毕业设计主要着眼于醋酐精馏工段的工艺设计，分为说明书、计算书、图纸等三大部分。在设计的过程中，参考了吉化电石厂醋酐装置的现有流程及设备，计算部分的主要依据是质量守恒定律和能量守恒定律；设备计算主要以《化工原理》为依据，参考了醋酐车间的现有设备的数据。 毕业设计是二学历学习的最后一个阶段，主要是对我们所学知识的一个全面检验，培养我们在思维、计算、绘图等方面的一个整体认识，为今后工作打下良好基础。 在本毕业设计中，操作控制采用DCS集中控制，效率高，损耗少，产品质量稳定；流量表安装在调解阀之前，介质相态稳定，确保仪表运行稳定。 本设计的重点是醋酐精馏塔，通过计算，合理选择了浮阀塔作为醋酐精馏塔，回流比10.453，理论板数25块，实际板数44块，进料板位置第12块，塔径0.800m，塔高15.6m，精馏段浮阀个数42个，提馏段浮阀个数27个，精馏段操作弹性1.86，提馏段操作弹性塔顶温度107.8℃，进料温度124.2℃，塔釜温度 关键词： 醋酐；精馏；物料守恒 Abstract The graduation design focus on acetic anhydride distillation section of process design, brochures, books, drawings and calculations. In the design, the reference to jihua Carbide factory acetic anhydride installations existing processes and equipment, the main part of the calculation is based on the law of conservation of mass and energy conservation; device to calculate mainly in chemical engineering, reference to the existing acetic anhydride workshop. Graduation is a second degree in the final stage of the study, mainly on what we have learned a comprehensive inspection, cultivating our thinking, calculations, drawings and other aspects of an overall awareness, to lay a good foundation for future work. In this thesis, operation control adopts DCS centralized control, high efficiency, low loss, product quality stability; flow valve installed in the conciliation phase stability before, the media, to ensure that the meter is running stable. The design focuses on acetic anhydride, distillation, by calculating the float valve selection as acetic anhydride distillation Tower, reflux ratio 10.453, theoretical plate number 25 blocks, the actual number of plates, feed 44 block position 12 block, diameter 0.800m, Tower high 15.6m, distillation segment valve number 42, stripping f