毕业论文(设计)-《掺杂多孔二氧化钛光催化性能评价条件研究》.docVIP

攀枝花学院本科毕业设计（论文） 摘要 l PAGE 1 ll 攀枝花学院本科毕业设计（论文） 掺杂多孔二氧化钛光催化性能评价条件研究 院 （系）： 生物与化学工程 年级专业： 化学工程与工艺 指导教师： 副教授 年六月 攀枝花学院本科毕业设计（论文） 目录 l PAGE 1 摘 要 近年来，二氧化钛半导体光催化剂在大气污染处理，污水处理等领域的应用得到迅速发展，已成为当前最有应用潜力的一种光催化剂。 本论文主要以合成制备出的掺杂多孔二氧化钛作为催化剂，研究其对亚甲基蓝的光催化性能，通过自制的光催化反应器，研究并探讨不同掺钒量、热处理温度等因素对多孔催化剂材料性能的影响，重点分析探讨了硫掺杂量对其结构和性能的影响，探讨物质结构与性能之间的关系。 本实验主要的研究手段：利用XRD观察其结晶形态，红外扫描测得其粒度分布，利用低温氮吸附法测定比表面积，并分析探讨不同因素对多孔二氧化钛光催化降解亚甲基蓝的影响。掺钒会降低其光催化性能，而硫的掺入则提高了其光催化性能。热处理温度会影响其晶型，进而影响其光催化性能，所得产品为锐钛型，而此晶型是光催化效果最好的状态。比表面积的大小也会影响其光催化性能，一般大的比表面积，其光催化性能就比较高。 关键词：多孔二氧化钛；光催化降解；硫含量；亚甲基蓝 ABSTRACT英语翻译与应用水平还需极大提高 英语翻译与应用水平还需极大提高 The semiconductor titanium dioxide has developed rapidly and become the most potential photocatalyst in recent years, due to its wide applications in air pollution and sewage treatment, etc. The photocatalytic performances of the as-prepared doping porous titania on methylene blue was investgated via slef-made photocatalytic reactor, and the factors such as vanadium dosage, heattreatment temperature affecting on the structure and its performance were also discussed, especially on the sulfur dosage . The major means of experimental study：observe the crystallization with XRD patterns, infrared scan gets particle size distribution, the use of low-temperature nitrogen adsorption specific surface area determination and analysis of different factors on the porous titanium dioxide photocatalytic degradation of methylene blue affected. Vanadium-doped reduce its photocatalytic properties, and the incorporation of sulfur is to improve its photocatalytic properties. Heat treatment temperature will affect its crystalline form, thereby affecting its photocatalytic properties, derived from anatase products, and this crystal form is the best photocatalytic state. Specific surface area will also affect the size of its photocatalytic properties,