毕业论文设计《超临界萃取秋刀鱼鱼油的研究》.docVIP

l 2013年度本科生毕业论文 超临界萃取秋刀鱼鱼油的研究 学 院： 理工学院 专 业： 化 学 年 级： 2009级 学生姓名： xxxxx 　 学 号： xxxxxxx 导师及职称： xxx（教授） 2013年5月 2013 Annual Graduation Thesis (Project) of the College Undergraduate Study on the Extraction of Oil from Saury by Supercritical Fluid Department: School of Science and Technology Major: Chemistry Grade: Student’s Name: Student No.: Tutor: Finished by May, 2013  摘要 目前，国内对鱼油提取的研究采用蒸煮法、淡碱水解法、酶解法、超临界萃取技术来获取鱼油的浓缩物，但前三种方法存在产品得率低、产量低、产品质量下降等；但超临界流体萃取技术的提油率最高，对鱼油的功能成分破坏最小。 超临界流体萃取技术就是利用超临界流体做萃取剂，从液体或固体中萃取出某些成分并进行分离的技术。超临界二氧化碳的高渗透性、高扩散性、低黏性，使其具有传质快和萃取速度高等优点；二氧化碳不燃、安全、无毒、对环境污染最少，并能从萃取物中挥发掉，不会留下溶解性残余物，从而得到安全而纯净的萃取物。 采用超临界二氧化碳萃取技术对秋刀鱼鱼油进行萃取，并探讨最佳工艺条件。实验结果表明，超临界二氧化碳萃取秋刀鱼鱼油的最佳工艺条件是萃取温度45℃、萃取压力27MPa、萃取时间2:30h、CO2流量15ml/Min。此条件下鱼油得率为1.4352 %，所得到鱼油是具有鱼腥气味、透明的淡黄色油状物。 关键词：秋刀鱼；超临界萃取法；鱼油；最佳条件 abstract At present， the main methods of producing fish oil are cooking，light alkaline hydrolysis， enzymatic hydrolysis and supercritical extraction and so on. While the former three methods have disadvantages like low product yield, low production, poor product quality, etc. The supercritical fluid extraction technology has the highest extraction rate and the lowest damage of the fish oil. SFE technology is a separation technology which uses supercritical fluid as extraction agent to extract and separate certain ingredients from liquid or solid. Supercritical gases, also known as supercritical fluid (SF), has high permeability, high diffusivity,and low viscosity which contributes to its fast mass transfer and high extraction speed. Carbon dioxide is non-combustible, safe, nontoxic and leaves least pollution to the environment. Therefore, it can obtain safe and pure extracts. My study focus on using SFE technology to extract fish oil from saury and the optimum technological conditions. The experiment shows that the optimum process conditions