离子色谱法测定食品中草铵膦-食品安全质量检测学报.PDF

7 5 Vol. 7 No. 5 2016 5 Journal of Food Safety and Quality May , 2016 林森煜, 黄嘉乐, 李秀英, 郭新东* (, 511447) 摘 要: 目的 方法 , Dionex OnGuard RP Dionex OnGuard Ag/H , IonPac AS11-HC (AG11-HC ), KOH (EG), , 结果 0.02~6.25 mg/L2.00~62.5 mg/L , 0.999, GlyGluf AMPA 0.0470.033 0.520 mg/kg, 0.160.11 1.73 mg/kg, 80.1% ~ 109%, (n=6)0.91%~12.5%, (n=5) 10.0%结论 , , GB 2763-2014 关键词: ; ; ; ; Determination of glyphosate glufosinate and (aminomethyl) phosphonic acid residues by ion chromatography * LIN Sen-Yu, HUANG Jia-Le, LI Xiu-Ying, GUO Xin-Dong (Guangzhou Quality Supervision and Testing Institute, Guangzhou 511447, China) ABSTRACT: Objective To establish a rapid, simple and simultaneous analytical method for the determination of glyphosate (Gly), glufosinate (Gluf) and (aminomethyl)phosphonic acid (AMPA) residues in food by ion chromatography. Method The amino acid and protein in food were precipitated with acetonitrile. The impurities and Cl- in the supernatant were removed by a Dionex OnGuard Ⅱ RP column and a Dionex OnGuard Ⅱ Ag/H column, respectively. The