（毕业学术论文设计）-年产2000吨磺基琥珀酸双己酯钠的车间的初步设计.docVIP

PAGE 摘 要 本设计主要是关于年产2000吨磺基琥珀酸双己酯钠的车间的初步设计。通过生产方法比较以及查阅大量的文献资料，选择了工艺路线，即先酯化再磺化。先在常压下由顺酐和正己醇反应生成马来酸双酯，再由马来酸双酯和亚硫酸氢钠在常压下反应生成磺基琥珀酸双己酯钠盐。完成了工艺流程设计，设备布置设计，主体设备设计。确定了工艺参数即反应釜的内径、高度、壁厚及零部件。通过物料衡算、热量衡算和设备计算对蒸馏塔、泵等辅助设备进行选型。依据化工厂的设计原则，对车间和设备进行了合理的平面和立面布置。同时对自动控制、公用工程及三废的产生和处理情况作了详细的论述。最后，绘制了带控制点的工艺流程图、反应釜的装配图和车间及设备的平立面布置图，完成了毕业设计说明书的撰写。 关键词：磺基琥珀酸双酯钠; 反应釜; 衡算; 设计 Abstract This design is about the preliminary reactor design of the annual output of 2000 tons of Sodium Dihenyl Sulfosuccinate.Thrugh productin methd comparison as well as consult massive literature material,has chosen the craft route,namely first esterificatin again sulfonatin.First,under the atmospheric pressure the maletic anhydride and the hexyl alohol responds to prduce maletic diester;Then through maletic diester and the Sodium bisulfite under the atmospheric pressure responds to produce Sodium dihexy Sulfosuccinate.According to process parameters, the reactor’s diameter, height, thickness and Components was determined. The heat exchangers, pumps and other ancillary equipment were choosed by material balance, energy balance and calculation of equipment. Based on the design principles of the chemical plants, the planar and vertical layout of the workshop and equipment was completed. Meanwhile, the automatic control, public works and the waste generation and treatment was exposed comprehensively. Finally, the chart of the process flow the control point, reactor assembly, planar and vertical layout of the workshop and equipment was drawed and the graduation brochures were completed. Key words：Lauric；Secondary Amine；Reactor Balance; Layout Design 目录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc201143732 摘 要 PAGEREF _Toc201143732 \h I HYPERLINK \l _Toc201143733 Abstract PAGEREF _Toc201143733 \h II HYPERLINK \l _Toc201143734 第1章 总 论 PAGEREF _Toc201143734 \h 1 HYPERLINK \l _Toc201143735 1.1 概述 PAGEREF _Toc201143735 \h 1 HYPERLINK \l _Toc201143736 1.1.1 意义与作用 PAGEREF _Toc201143736 \h 1 HYPERLINK \l _Toc20