《110万吨年焦化厂硫铵工段的工艺设计》-毕业论文.doc

l 唐 山 学 院 毕 业 设 计 设计题目：110万吨/年焦化厂硫铵工段的工艺设计 系 别： 环境与化学工程系 班 级： 10生物化工工艺 （1） 班 姓　 　名： 指 导 教 师： 2013 年6 月6 日 110万吨/年焦化厂硫铵工段的工艺设计 摘要 本设计为年产焦炭110万吨焦化厂回收车间硫铵工段的工艺设计,该焦化厂拟建唐山市京唐港.本设计内容包括:生产原理、工艺流程、计算及设备的选型等。本设计采用技术成熟的饱和器法中半直接法来回收煤气中的氨 工艺流程如下：从冷凝工段来得煤气首先进入煤气预热器，然后进入饱和器，在饱和器内，煤气中的氨与硫酸反应生产硫铵，硫铵经后续操作分离，从饱和器出来的煤气经除酸器后送往粗苯工段。 工艺计算包括饱和器的物料和热量平衡计算，通过计算来确定母液的适宜温度和煤气预热温度。同时根据本设计的规模，对工段的工艺布置原则作了简要说明，对工段生产操作也作了简要说明，对非工段部分提出了一些具体要求，通过岗位操作定员知道本工段需要职工人员数。 本设计根据设计规模，对工艺布置和操作流程做了简要说明，对非工艺部分提出了一些具体要求，此外还给出了图纸目录说明和设备一览表。 关键词：焦炭饱和器氨硫铵 硫铵工段。 1.1 million tons/year plant ammonium sulphate process design section Abstract This design is an annual output of 1.1 million tons of coke plant recycling ammonium sulphate workshop section of process design. The coking plant proposed tangshan jingtang. This design content including: Production principle, process flow, calculation and equipment selection, etc. This design adopts the mature technology of the saturator method in half a direct method for recovery of ammonia gas. The process flow is as follows: Comes from the condensation section in gas into the gas preheater in the first place,.Then enter the saturator. Within the saturator. Gas ammonia reaction with sulfuric acid in the production of ammonium sulphate. Ammonium sulphate with subsequent separation operation. Out of the saturator gas after deacidification is sent to the crude benzol section. Process calculation including the saturator of material and heat balance calculation. Through calculation of mother liquid to determine the optimum temperature and the gas preheating temperature. According to the size of this design at the same time. Layout principle of the technology of section gave a brief description, also gave a brief explanation to section production operation, puts forward some concrete requirements for the section part, through post operation complemen