原创力文档Highly Ordered Porous Anodic Alumina with Large Diameter Pores Fabricated by an Improved Two-Step Anodization Approach-学术期刊.pdf
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Article
Journal of
Nanoscience and Nanotechnology
Copyright © 2015 American Scientific Publishers
Vol. 15, 1725–1731, 2015
All rights reserved
Printed in the United States of America /jnn
Highly Ordered Porous Anodic Alumina with
Large Diameter Pores Fabricated by an
Improved Two-Step Anodization Approach
∗
Xiaohong Li, Siyu Ni , and Xingping Zhou
College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, Shanghai 201620, P. R. China
The aim of this study is to prepare highly ordered porous anodic alumina (PAA) with large pore sizes
( 200 nm) by an improved two-step anodization approach which combines the first hard anodiza-
tion in oxalic acid–water–ethanol system and second mild anodization in phosphoric acid–water–
ethanol system. The surface morphology and elemental composition of PAA are characterized by
field emission scanning electron microscopy (FESEM) and energy-dispersive X-ray spectrometer
(EDS). The effects of matching of two-step anodizing voltages on the regularity of pore arrangement
is evaluated and discussed. Moreover, the pore formation mechanism is also
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