烧结温度对泡沫铌力学性能及微观组织的影响-中国有色金属学报.PDFVIP

第 20 卷第 10 期 中国有色金属学报 2010 年 10 月 Vol.20 No.10 The Chinese Journal of Nonferrous Metals Oct. 2010 文章编号：1004-0609(2010)10-2014-05 烧结温度对泡沫铌力学性能及微观组织的影响 节云峰，阮建明，邹俭鹏 ( 中南大学 粉末冶金国家重点实验室，长沙 410083) 摘 要：采用新型泡沫浸渍法制备具有较高强度和良好生物相容性的泡沫铌。利用 SEM、 XRD 和 CS600 碳硫 测试仪分析泡沫铌的微观结构、形貌及相组成，同时对多孔材料的孔隙结构和力学性能进行分析。结果表明：制 备的泡沫铌具有与人体松质骨相似的三维、连通孔隙结构，其碳含量为 0.049%(质量分数) ；泡沫铌的抗压强度随 着烧结温度的升高先增加后降低，而弹性模量随着烧结温度的升高而增大；烧结温度为 1 750 ℃时，其抗压强度 为 36.69 MPa，弹性模量为 0.815 GPa，与人体松质骨的力学性能相匹配。 关键词：泡沫铌；浸渍；烧结温度；力学性能 中图分类号：TG 146.4 文献标志码：A Effect of sintering temperature on mechanical properties and microstructure of Nb foams JIE Yun-feng, RUAN Jian-ming, ZOU Jian-peng (State Key laboratory of Powder Metallurgy, Central South University, Changsha 410083, China) Abstract: Nb foams with high strength and excellent biocompatibility were prepared by a novel foam dipping. SEM, XRD and CS600 carbon and sulfur analyzer were used to characterize the microstructures, morphologies and phase constituents, respectively. And the mechanical properties and pore structures were also analyzed. The results show that the Nb foams have three-dimensional, connected pore structure, and the carbon content is 0.049% (mass fraction). The pure phase in the porous niobium-based materials was prepared by solid phase sintering, which is similar to the structure of cancellous bone. With sintering temperature increasing, the compressive strength increases and then reduces, while the elastic modulus increases with the sintering temperature increasing. When the sintering temperature is 1